Derivative spectrophotometric determination of droperidol in presence of parabens

被引：17

作者：

Trabelsi, H ^{[1
]}

Raouafi, F ^{[1
]}

Limam, M ^{[1
]}

Bouzouita, K ^{[1
]}

机构：

[1] Lab Natl Controle Medicaments, Tunis, Tunisia

来源：

JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS | 2002年 / 29卷 / 1-2期

关键词：

droperidol; neuroleptic; derivative spectrophotometry;

D O I：

10.1016/S0731-7085(02)00095-X

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

We have developed a fast and accurate method for the determination of droperidol in the presence of methylparaben and propylparaben using derivative spectrophotometry. The first derivative amplitudes at 255.2 nm were selected for the assay. Calibration graph follows Beer's law in the range of 5-35 mug ml(-1). The coefficient of variation (CV) for intra-day and inter-day precision were less than 1.0 and 2.0%, respectively. The method was applied in the quality control of commercial oral and injection solutions and proved to be suitable for routine analysis. (C) 2002 Elsevier Science B.V. All rights reserved.

引用

页码：239 / 245

页数：7

共 50 条

[31] Third order derivative spectrophotometric determination of ascorbic acid in fruits and vegetables
Ozgur, MU
Sungur, S
TALANTA, 1995, 42 (11) : 1631 - 1640
[32] Derivative spectrophotometric determination of ruthenium(M) using cinnamaidehyde isonicotinoylhydrazone (CINH)
Kumar, V. Kiran
Rao, M. Rameswara
Chandrasekhar, K. B.
Devanna, N.
ASIAN JOURNAL OF CHEMISTRY, 2008, 20 (03) : 2197 - 2204
[33] DERIVATIVE SPECTROPHOTOMETRIC ASSAY OF ACETAMINOPHEN AND SPECTROFLUOROMETRIC DETERMINATION OF ITS MAIN IMPURITY
MILCH, G
SZABO, E
JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 1991, 9 (10-12) : 1107 - 1113
[34] Second and Third Derivative Spectrophotometric Determination of Liothyronine and Thyroxine in Human Serum
Fakhre, Nabil A.
Riasheed, Chnar M.
Ali, Dashty Kh
EGYPTIAN JOURNAL OF CHEMISTRY, 2021, 64 (11): : 6385 - 6397
[35] SIMULTANEOUS 2ND-DERIVATIVE SPECTROPHOTOMETRIC DETERMINATION OF MANGANESE AND COPPER
FERNANDEZALBA, AR
MARTINEZVIDAL, JL
AGUILERA, P
FRENICHE, F
AGUERA, A
ANALYTICAL LETTERS, 1992, 25 (08) : 1581 - 1593
[36] Derivative Spectrophotometric Determination of Adapalene in its Bulk and Pharmaceutical Dosage Form
Adhikari, Lopamudra
Jagadev, Sarbeswar
Sahu, Sanjib
Moitra, S. K.
Murthy, P. N.
ASIAN JOURNAL OF CHEMISTRY, 2012, 24 (03) : 1094 - 1096
[37] Fourth order derivative spectrophotometric determination of benzyl alcohol in piroxicam injections
Rizk, M.
Ibrahim, F.
Hefnawy, M.
Nasr, J. J.
JOURNAL OF THE CHINESE CHEMICAL SOCIETY, 2006, 53 (04) : 767 - 772
[38] Derivative spectrophotometric determination of copper and palladium simultaneously by using MDTC as a reagent
Kaur, Varinder
Malik, Ashok Kumar
Verma, Neelam
ANALYTICAL LETTERS, 2007, 40 (12) : 2360 - 2373
[39] DIRECT DERIVATIVE SPECTROPHOTOMETRIC DETERMINATION OF NITRAZEPAM AND CLONAZEPAM IN BIOLOGICAL-FLUIDS
RANDEZGIL, F
DAROS, JA
SALVADOR, A
DELAGUARDIA, M
JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 1991, 9 (07) : 539 - 545
[40] Development and Validation of a Derivative Spectrophotometric Method for Simultaneous Determination of Simvastatin and Ezetimibe
Souri, Effat
Amanlou, Masoud
E-JOURNAL OF CHEMISTRY, 2010, 7 : S197 - S202

← 1 2 3 4 5 →