Gelatin-assisted green synthesis of bismuth sulfide nanorods under microwave irradiation

被引：25

作者：

Xue, Bin ^{[1
]}

Sun, Tao ^{[1
]}

Mao, Fang ^{[1
]}

Xie, Jing ^{[1
]}

机构：

[1] Shanghai Ocean Univ, Coll Food Sci & Technol, Dept Chem, Shanghai 201306, Peoples R China

来源：

MATERIALS LETTERS | 2014年 / 122卷

关键词：

Bismuth sulfide; Nanorods; Green synthesis; Crystal growth; FACILE SYNTHESIS; HYDROTHERMAL SYNTHESIS; BI2S3; NANORODS; NANOPARTICLES; MICROSPHERES; NANOWIRES;

D O I：

10.1016/j.matlet.2014.02.013

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Bismuth sulfide (Bi2S3) nanorods were synthesized by a gelatin-assisted green solution process under microwave irradiation. The crystal phase, morphology and optical properties of the as-synthesized Bi2S3 nanorods were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), UV-vis diffuse reflection spectroscopy (UV-vis DRS) and photoluminescence (PL) spectroscopy. On the basis of the morphological evolution processes, the growth mechanism of the as-synthesized Bi2S3 nanorods was discussed. The as-synthesized Bi2S3 nanorods exhibited a strong excitonic absorbance in UV-vis DRS and a strong emission peak in PL spectrum. The gelatin-assisted synthesis approach under microwave irradiation is green, facile and efficient thus promoting large-scale production and application of Bi2S3 nanorods in photoelectric nanodevice and other fields. (C) 2014 Elsevier B.V. All rights reserved.

引用

页码：106 / 109

页数：4

共 20 条

[1] Facile synthesis of Bi2S3 hierarchical nanostructure with enhanced photocatalytic activity [J].

Chen, Fengjuan ;

Cao, Yali ;

Jia, Dianzeng .

JOURNAL OF COLLOID AND INTERFACE SCIENCE, 2013, 404 :110-116

[2] Shape-controlled solvothermal synthesis of Bi2S3 for photocatalytic reduction of CO2 to methyl formate in methanol [J].

Chen, Jingshuai ;

Qin, Shiyue ;

Song, Guixian ;

Xiang, Tianyu ;

Xin, Feng ;

Yin, Xiaohong .

DALTON TRANSACTIONS, 2013, 42 (42) :15133-15138

[3] Synthesis and assembly of Bi2S3 nanoparticles at the water-toluene interface [J].

Fan, Dongbo ;

Thomas, P. John ;

O'Brien, Paul .

CHEMICAL PHYSICS LETTERS, 2008, 465 (1-3) :110-114

[4] Gelatin-assisted hydrothermal synthesis of single crystalline zinc oxide nanostars and their photocatalytic properties [J].

Fang, Ke-Ming ;

Wang, Zhen-Zhen ;

Zhang, Ming ;

Wang, Ai-Jun ;

Meng, Zi-Yan ;

Feng, Jiu-Ju .

JOURNAL OF COLLOID AND INTERFACE SCIENCE, 2013, 402 :68-74

[5] ZnO-based hollow microspheres: Biopolymer-assisted assemblies from ZnO nanorods [J].

Gao, Shuyan ;

Zhang, Hongjie ;

Wang, Xiaomei ;

Deng, Ruiping ;

Sun, Dehui ;

Zheng, Guoli .

JOURNAL OF PHYSICAL CHEMISTRY B, 2006, 110 (32) :15847-15852

[6] Preparation of uniform Bi2S3 nanorods using xanthate complexes of bismuth(III) [J].

Han, Qiaofeng ;

Chen, Jian ;

Yang, Xujie ;

Lu, Lude ;

Wang, Xin .

JOURNAL OF PHYSICAL CHEMISTRY C, 2007, 111 (38) :14072-14077

[7] Growth of bismuth sulfide nanowire using bismuth trisxanthate single source precursors [J].

Koh, YW ;

Lai, CS ;

Du, AY ;

Tiekink, ERT ;

Loh, KP .

CHEMISTRY OF MATERIALS, 2003, 15 (24) :4544-4554

[8] Synthesis of anatase TiO2 nanoparticles with β-cyclodextrin as a supramolecular shell [J].

Li, Landong ;

Sun, Xiaohong ;

Yang, Yali ;

Guan, Naijia ;

Zhang, Fuxiang .

CHEMISTRY-AN ASIAN JOURNAL, 2006, 1 (05) :664-668

[9] Selected-control hydrothermal synthesis and photoresponse properties of Bi2S3 micro/nanocrystals [J].

Li, Yanping ;

Wei, Feng ;

Ma, Yaoguang ;

Zhang, Hui ;

Gao, Zhiwei ;

Dai, Lun ;

Qin, Guogang .

CRYSTENGCOMM, 2013, 15 (33) :6611-6616

[10] Wet chemical synthesis of Bi2S3 nanorods for efficient photocatalysis [J].

Luo, Yongfeng ;

Chen, Hong ;

Li, Xi ;

Gong, Zhiqiang ;

Wang, Xinjun ;

Peng, Xiaofang ;

He, Mengdong ;

Sheng, Zhongzhi .

MATERIALS LETTERS, 2013, 105 :12-15

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