Microwave-Assisted Carbonyl-Carbonyl Coupling Route for the Preparation of a Useful Intermediate in the Synthesis of Carbapenems

被引：3

作者：

Xia, Zhining ^{[2
]}

Long, Sha ^{[2
]}

Xiao, Shangyou ^{[2
]}

Zou, Xiaoping ^{[2
]}

D'Aurizio, Antonio ^{[1
]}

Panunzio, Mauro ^{[1
]}

机构：

[1] CNR, ISOF, Dept Chem, I-40126 Bologna, Italy

[2] Chongqing Univ, Inst Chem & Chem Engn, Chongqing 630044, Peoples R China

来源：

SYNTHETIC COMMUNICATIONS | 2009年 / 39卷 / 12期

关键词：

Carbapenem; imipenem; MAOS (microwave-assisted organic synthesis); phosphite-mediated cyclization; Wittig intramolecular reaction; CYCLIZATION REACTION; PENEMS;

D O I：

10.1080/00397910802638586

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Microwave-assisted organic synthesis has been used for the cyclization of a monocyclic oxoamide to the corresponding bicyclic derivative via a Wittig-type coupling by means of phosphite reagents. The parameters influencing the reaction yields under microwave (dielectric heating) and classical conditions (convective heating) have been evaluated.

引用

页码：2151 / 2160

页数：10

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