Microwave and conventional sintering of the SiC/SiC composites: The densification and pore distributions

被引:11
作者
Yang, Huiyong [1 ]
Zhou, Xingui [1 ]
Yu, Jinshan [1 ]
Wang, Honglei [1 ]
Huang, Zelan [2 ]
机构
[1] Natl Univ Def Technol, Coll Aerosp Sci & Engn, Sci & Technol Adv Ceram Fibers & Composites Lab, Changsha 410073, Hunan, Peoples R China
[2] Chongyi Zhangyuan Tungsten Co Ltd, Ganzhou 341000, Peoples R China
关键词
Ceramics; Composite materials; Sintering; Microstructure; MECHANICAL-PROPERTIES; BLANKET DESIGNS; SILICON-CARBIDE; POLYCARBOSILANE; BEHAVIOR;
D O I
10.1016/j.jallcom.2015.12.085
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
SiC/SiC composites were fabricated by polymer impregnation and pyrolysis (PIP) process via microwave and conventional heating at 800 degrees C, 900 degrees C, 1000 degrees CC and 1100 degrees C. The effects of sintering heating types and sintering temperatures on the densification process and pore distributions of the fabricated SiC/SiC composites were studied. The densification processes were discussed in the form of the weight gain rates at each PIP cycle. The pore location distributions were observed by scanning electron microscopy (SEM) and computed tomography (CT) technique. The porosity and pore size distributions were quantified by the mercury intrusion test. The results indicate that lower heating rates and higher sintering temperatures are benefit to the densification of the SiC/SiC composites. But the more micro-cracks generated from higher heating rates of microwave sintering (similar to degrees 40 degrees C/min) make the flexural strength and toughness of the SiC/SiC composites higher than that of the conventional sintered ones. (C) 2015 Elsevier B.V. All rights reserved.
引用
收藏
页码:252 / 258
页数:7
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