Synthesis and characterisation of VG nanosheets on silica aerogel by plasma-enhanced chemical vapour deposition method

被引:2
作者
Vigneswari, S. [1 ]
Murugesan, S. [1 ]
机构
[1] Sathyabama Inst Sci & Technol, Dept Phys, Chennai 600119, Tamil Nadu, India
关键词
Raman spectra; nanostructured materials; atomic force microscopy; X-ray diffraction; plasma CVD; scanning electron microscopy; surface morphology; nanofabrication; graphene; AFM; cross-sectional SEM; silica aerogel; plasma-enhanced chemical vapour deposition method; silicon substrate; physiochemical properties; Raman spectroscopy; vertical graphene nanosheets; full wave half maximum; temperature; 800; 0; degC; pressure; 1; atm; SiO2; C; REDUCED GRAPHENE OXIDE; GROWTH; ENERGY; LAYER;
D O I
10.1049/mnl.2018.5436
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Vertical graphene (VG) nanosheets are directly grown on silica aerogel and silicon substrate (100) by plasma-enhanced chemical vapour deposition process in the presence of hydrogen as a reducing agent at atmospheric pressure at 800 degrees C. The physiochemical properties of the nanohybrid were thoroughly characterised by Raman spectroscopy, scanning electron microscopy (SEM) and atomic force microscopy (AFM). The presence of full wave half maximum of D, G and D ' indicates VG nanowalls. The height (50 nm) of the VG nanowalls were confirmed by SEM and Raman spectroscopy but AFM reveals it as 15 nm. Surface and cross-sectional SEM show the uniform distribution of vertical growth of nanowalls and the AFM revealed surface morphology of VG nanowalls.
引用
收藏
页码:595 / 599
页数:5
相关论文
共 24 条
[1]   Facile One-Pot Synthesis of Graphene Oxide by Sonication Assisted Mechanochemical Approach and Its Surface Chemistry [J].
Bera, Madhab ;
Chandravati ;
Gupta, Pragya ;
Maji, Pradip K. .
JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, 2018, 18 (02) :902-912
[2]   Emerging energy and environmental applications of vertically-oriented graphenes [J].
Bo, Zheng ;
Mao, Shun ;
Han, Zhao Jun ;
Cen, Kefa ;
Chen, Junhong ;
Ostrikov, Kostya .
CHEMICAL SOCIETY REVIEWS, 2015, 44 (08) :2108-2121
[3]   Hallmark of perfect graphene [J].
Duplock, EJ ;
Scheffler, M ;
Lindan, PJD .
PHYSICAL REVIEW LETTERS, 2004, 92 (22) :225502-1
[4]   Raman spectrum of graphene and graphene layers [J].
Ferrari, A. C. ;
Meyer, J. C. ;
Scardaci, V. ;
Casiraghi, C. ;
Lazzeri, M. ;
Mauri, F. ;
Piscanec, S. ;
Jiang, D. ;
Novoselov, K. S. ;
Roth, S. ;
Geim, A. K. .
PHYSICAL REVIEW LETTERS, 2006, 97 (18)
[5]   Micro- and nanoscale electrical characterization of large-area graphene transferred to functional substrates [J].
Fisichella, Gabriele ;
Di Franco, Salvatore ;
Fiorenza, Patrick ;
Lo Nigro, Raffaella ;
Roccaforte, Fabrizio ;
Tudisco, Cristina ;
Condorelli, Guido G. ;
Piluso, Nicolo ;
Sparta, Noemi ;
Lo Verso, Stella ;
Accardi, Corrado ;
Tringali, Cristina ;
Ravesi, Sebastiano ;
Giannazzo, Filippo .
BEILSTEIN JOURNAL OF NANOTECHNOLOGY, 2013, 4 :234-242
[6]  
Fu CJ, 2013, INT J ELECTROCHEM SC, V8, P6269
[7]   Enhanced hydrophilicity and salt rejection study of graphene oxide-polysulfone mixed matrix membrane [J].
Ganesh, B. M. ;
Isloor, Arun M. ;
Ismail, A. F. .
DESALINATION, 2013, 313 :199-207
[8]   Nanolithography and manipulation of graphene using an atomic force microscope [J].
Giesbers, A. J. M. ;
Zeitler, U. ;
Neubeck, S. ;
Freitag, F. ;
Novoselov, K. S. ;
Maan, J. C. .
SOLID STATE COMMUNICATIONS, 2008, 147 (9-10) :366-369
[9]   Spatially resolved raman spectroscopy of single- and few-layer graphene [J].
Graf, D. ;
Molitor, F. ;
Ensslin, K. ;
Stampfer, C. ;
Jungen, A. ;
Hierold, C. ;
Wirtz, L. .
NANO LETTERS, 2007, 7 (02) :238-242
[10]   HELICAL MICROTUBULES OF GRAPHITIC CARBON [J].
IIJIMA, S .
NATURE, 1991, 354 (6348) :56-58