A green chemical route for the synthesis of Mn3O4 nanoparticles

被引：34

作者：

Durmus, Zehra ^{[1
]}

Kavas, Hueseyin ^{[2
]}

Baykal, Abdulhadi ^{[1
]}

Toprak, Muhammet S. ^{[3
]}

机构：

[1] Fatih Univ, Dept Chem, TR-34500 Istanbul, Turkey

[2] Fatih Univ, Dept Phys, TR-34500 Istanbul, Turkey

[3] Royal Inst Technol, Funct Mat Div, SE-16440 Stockholm, Sweden

来源：

CENTRAL EUROPEAN JOURNAL OF CHEMISTRY | 2009年 / 7卷 / 03期

关键词：

Ionic liquids; Nanoparticles; Mn3O4; BMIM]OH; TEM; EPR; TEMPERATURE IONIC LIQUID; NANOCRYSTALS; OXIDES; CO3O4;

D O I：

10.2478/s11532-009-0049-4

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A novel environmental friendly, room temperature route using an ionic liquid 1-n-butyl-3-methylimidazolium hydroxide ([BMIM]OH) for the synthesis of Mn3O4 nanoparticles is presented. The product was characterized using Fourier transform infrared spectroscopy, X-ray powder diffraction, and transmission electron microscopy. Phase purity was confirmed by XRD, and X-ray line profile fitting determined a crystallite size of 42 +/- 11 nm. TEM analysis revealed various morphologies. EPR measurements have indicated the existence of long-range interactions, due to the wide range of particle sizes and morphologies observed

引用

页码：555 / 559

页数：5

共 33 条

[1] Synthesis of layered LiMnO2 as an electrode for rechargeable lithium batteries [J].