Precipitation behavior of type 347H heat-resistant austenitic steel during long-term high-temperature aging

被引:27
作者
Zhou, Yinghui [1 ]
Li, Yanmo [1 ]
Liu, Yongchang [1 ]
Guo, Qianying [1 ]
Liu, Chenxi [1 ]
Yu, Liming [1 ]
Li, Chong [1 ]
Li, Huijun [1 ]
机构
[1] Tianjin Univ, Sch Mat Sci & Engn, State Key Lab Hydraul Engn Simulat & Safety, Tianjin 300072, Peoples R China
基金
中国国家自然科学基金; 国家高技术研究发展计划(863计划);
关键词
STAINLESS-STEEL; EVOLUTION; CREEP; CARBIDE; TOUGHNESS; EXPOSURE; PHASE; M23C6; MX;
D O I
10.1557/jmr.2015.343
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The microstructural evolution of type 347H heat-resistant austenitic steel during long-term aging at 700-900 degrees C was investigated by using a transmission microscope, a scanning electron microscope, and electron energy spectrum technology. The microstructural examination showed the typical micrographs of MX carbonitrides and M23C6 carbides after aging. The existence of the Z phase (NbCrN) at the grain boundaries during aging was identified. Meanwhile, the possible precipitation sequence of these particles was also confirmed. In the beginning of aging, fine Nb(C,N) precipitates first, then, M23C6 carbides precipitate along the grain boundaries. Finally, the Z phase is also observed at the grain boundaries. Moreover, the influence of isothermal holding temperature on the precipitation of MX carbonitrides and M23C6 carbides was discussed. The various microstructural characterizations showed that the M23C6 carbides and MX carbonitrides precipitate more easily with the increase of aging temperature. Furthermore, the number and the size of MX particles and M23C6 carbides increase when the isothermal holding time is prolonged.
引用
收藏
页码:3642 / 3652
页数:11
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