Chemical deposition of PbS on self-assembled monolayers of 16-mercaptohexadecanoic acid

被引：83

作者：

Meldrum, FC ^{[1
]}

Flath, J ^{[1
]}

Knoll, W ^{[1
]}

机构：

[1] MAX PLANCK INST POLYMER RES,D-55122 MAINZ,GERMANY

来源：

LANGMUIR | 1997年 / 13卷 / 07期

关键词：

D O I：

10.1021/la9608369

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The chemical deposition of PbS on self-assembled monolayers of 16-mercaptohexadecanoic acid formed on evaporated gold was investigated. In situ evaluation of the thickness of the crystalline film and of the kinetics of crystal growth was carried out by surface plasmon spectroscopy (SPS). The SPS measurements were correlated with structural and morphological data on the PbS films, as obtained by transmission electron microscopy and scanning electron microscopy, thus enabling the film structure at precise thicknesses to be identified. The applicability of SPS measurements to such a system was demonstrated. The microscopical analysis clearly showed that the film exhibited a marked structural change at a thickness of 25 nm. It was proposed that the film formed by an ion-by-ion mechanism.

引用

页码：2033 / 2049

页数：17

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