5-[(4-Acetylphenyl)aminomethylene]-2,2-dimethyl-1,3-dioxane-4,6-dione

被引：3

作者：

Li, Rui ^{[1
]}

Ding, Zhen-Yu ^{[1
]}

Wei, Yu-Quan ^{[1
]}

Ding, Jian ^{[2
]}

机构：

[1] Sichuan Univ, State Key Lab Biotherapy, W China Hosp, Chengdu 610041, Peoples R China

[2] Chinese Acad Sci, State Key Lab Drug Res, Shanghai Inst Mat Med, Shanghai 201203, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷

关键词：

D O I：

10.1107/S1600536809017425

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C(15)H(15)NO(5), the six-membered dioxane ring assumes an envelope conformation with the dimethyl substituted C atom as the flap atom. An intramolecular N-H center dot center dot center dot O interaction is also present. In the crystal structure the molecules are linked via C-H center dot center dot center dot O hydrogen bonds into supramolecular chains along the b axis.

引用

页码：O1297 / U2022

页数：8

共 6 条

[1] SYNTHESIS OF 4(1H)-QUINOLONES BY THERMOLYSIS OF ARYLAMINOMETHYLENE MELDRUM ACID-DERIVATIVES [J].

CASSIS, R ;

TAPIA, R ;

VALDERRAMA, JA .

SYNTHETIC COMMUNICATIONS, 1985, 15 (02) :125-133

[2]

Farrujia LJ., 1997, J APPL CRYSTALLOGR, V30, P565, DOI [10.1107/S0021889897003117, DOI 10.1107/S0021889897003117]

[3] NRCVAX - AN INTERACTIVE PROGRAM SYSTEM FOR STRUCTURE-ANALYSIS [J].

GABE, EJ ;

LEPAGE, Y ;

CHARLAND, JP ;

LEE, FL ;

WHITE, PS .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1989, 22 :384-387

[4]

GABE EJ, 1993, AM CRYST ASS M PITTS

[5] 5H-Dibenzo[c,h]1,6-naphthyridin-6-ones:: Novel topoisomerase I-targeting anticancer agents with potent cytotoxic activity [J].

Ruchelman, AL ;

Singh, SK ;

Ray, A ;

Wu, XH ;

Yang, JM ;

Li, TK ;

Liu, A ;

Liu, LF ;

LaVoie, EJ .

BIOORGANIC & MEDICINAL CHEMISTRY, 2003, 11 (09) :2061-2073

[6] A short history of SHELX [J].

Sheldrick, George M. .

ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122

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