First Profile of Phenolic Compounds from Maltese Extra Virgin Olive Oils Using Liquid-Liquid Extraction and Liquid Chromatography-Mass Spectrometry

被引:8
|
作者
Gatt, Lucienne [1 ,2 ]
Lia, Frederick [3 ]
Zammit-Mangion, Marion [1 ,2 ]
Thorpe, Simon J. [4 ]
Schembri-Wismayer, Pierre [5 ]
机构
[1] Univ Malta, Fac Med & Surg, Dept Physiol & Biochem, Msida, Malta
[2] Univ Malta, Ctr Mol Med & Biobanking, Msida, Malta
[3] Univ Malta, Fac Sci, Dept Chem, Msida, Malta
[4] Univ Sheffield, Dept Chem, Sheffield, S Yorkshire, England
[5] Univ Malta, Fac Med & Surg, Dept Anat, Msida, Malta
关键词
extra virgin olive oil; phenols; liquid-liquid extraction; Liquid Chromatography-Mass Spectrometry; ANTIOXIDANT; LIGNANS; COMPONENTS; QUALITY; CANCER;
D O I
10.5650/jos.ess20130
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
This study presents the profile of phenolic extracts from different Extra Virgin Olive Oils (EVOOs) from Malta and is the first study that characterizes the phenolic profile of the Maltese EVOOs Bidni (B) and Malti (M) using liquid-liquid extraction (LLE) and Liquid Chromatography-Mass Spectrometry (LC-MS). The total phenolic content (TPC), ortho diphenolic content (TdPC) and flavonoid content (TFC) were determined using the Folin-Ciocalteau assay, the Arnow's assay and the Aluminium Chloride method respectively. Results show that the B variety had the highest TPC, TdPC and TFC. Using LC-MS analysis, over 30 phenolic compounds were identified belonging to different classes of phenolic compounds.
引用
收藏
页码:145 / 153
页数:9
相关论文
共 50 条
  • [1] Application of Dispersive Liquid-Liquid Aerosol Phase Extraction to the Analysis of Total and Individual Phenolic Compounds in Fried Extra Virgin Olive Oils
    Sanchez, Raquel
    Sanahuja, Ana Beltran
    Moya, Maria Soledad Prats
    Todoli, Joseï-Luis
    JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2023, 71 (28) : 10742 - 10750
  • [2] Phenolic Compounds Profiling of Virgin Olive Oils from Different Varieties Cultivated in Mendoza, Argentina, by Using Liquid Chromatography Mass Spectrometry
    Monasterio, R. P.
    Olmo-Garcia, L.
    Bajoub, A.
    Fernandez-Gutierrez, A.
    Carrasco-Pancorbo, A.
    JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2017, 65 (37) : 8184 - 8195
  • [3] The Phenolic Fraction of Italian Extra Virgin Olive Oils: Elucidation Through Combined Liquid Chromatography and NMR Approaches
    Klikarova, Jitka
    Rotondo, Archimede
    Cacciola, Francesco
    Ceslova, Lenka
    Dugo, Paola
    Mondello, Luigi
    Rigano, Francesca
    FOOD ANALYTICAL METHODS, 2019, 12 (08) : 1759 - 1770
  • [4] Metabolic profiling approach to determine phenolic compounds of virgin olive oil by direct injection and liquid chromatography coupled to mass spectrometry
    Olmo-Garcia, Lucia
    Bajoub, Aadil
    Monasterio, Romina Paula
    Fernandez-Gutierrez, Alberto
    Carrasco-Pancorbo, Alegria
    FOOD CHEMISTRY, 2017, 231 : 374 - 385
  • [5] Determination of Forty Pollutants in Wastewater by Liquid-Liquid Extraction and Gas Chromatography-Mass Spectrometry
    Song, Guangqing
    Xi, Hongbo
    Zhou, Yuexi
    ANALYTICAL LETTERS, 2016, 49 (10) : 1480 - 1491
  • [6] Comprehensive Profiling of Phytohormones in Honey by Sequential Liquid-Liquid Extraction Coupled with Liquid Chromatography-Mass Spectrometry
    Wang, Qing
    Cai, Wen-Jing
    Yu, Lei
    Ding, Jun
    Feng, Yu-Qi
    JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2017, 65 (03) : 575 - 585
  • [7] Salting-out-assisted liquid-liquid extraction with acetonitrile for the determination of trimetazidine in rat plasma using liquid chromatography-mass spectrometry
    Xiong, Xin
    Yang, Li
    BIOMEDICAL CHROMATOGRAPHY, 2015, 29 (02) : 268 - 274
  • [8] Liquid-liquid extraction for the enrichment of edible oils with phenols from olive leaf extracts
    Japon-Lujan, R.
    De Castro, M. D. Luque
    JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2008, 56 (07) : 2505 - 2511
  • [9] Ultrasonic-assisted extraction method of phenolic compounds in Extra-Virgin Olive Oils (EVOOs) by Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry (UPLC-MS/MS)
    Kivrak, Seyda
    Kivrak, Ibrahim
    SEPARATION SCIENCE AND TECHNOLOGY, 2021, 56 (02) : 322 - 329
  • [10] The Phenolic Fraction of Italian Extra Virgin Olive Oils: Elucidation Through Combined Liquid Chromatography and NMR Approaches
    Jitka Klikarová
    Archimede Rotondo
    Francesco Cacciola
    Lenka Česlová
    Paola Dugo
    Luigi Mondello
    Francesca Rigano
    Food Analytical Methods, 2019, 12 : 1759 - 1770