Bis[1,3-bis(1-benzyl-1H-benzimidazol-2-yl)-2-oxapropane]zinc(II) dipicrate dimethylformamide disolvate

被引：8
|
作者：
Wu, Huilu [1 ]
Yun, Ruirui [1 ]
Li, Ke [1 ]
Tao, Sun [1 ]
Wang, Kaitong [1 ]
机构：
[1] Lanzhou Jiaotong Univ, Sch Chem & Biol Engn, Lanzhou 730070, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷
关键词：
D O I：
10.1107/S1600536809022296
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, [Zn(C(30)H(26)N(4)O)(2)](C(6)H(2)N(3)O(7))(2)center dot-2C(3)H(7)NO, the Zn(II) ion is coordinated in a distorted octahedral environment involving four equatorial N atoms and two O atoms in axial sites. The dihedral angles between the benzimidazole ring system and the phenyl rings in each of the benzylbenzimidazole units are 78.56 (12), 81.68 (11), 75.76 (10) and 85.78 (9)degrees. In the crystal structure, there are weak but significant intermolecular pi-pi stacking interactions with centroid-centroid distances of 3.685 (1) and 3.978 (1) angstrom.
引用
收藏
页码：M786 / U918
页数：21
相关论文
共 50 条
  • [1] 1,3-Bis(1-benzyl-1H-benzimidazol-2-yl)-2-oxapropane
    Wu, Huilu
    Yun, Ruirui
    Wang, Kaitong
    Huang, Xingcai
    Sun, Qingyu
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O1014 - U1947
  • [2] Bis[1,3-bis(1-benzyl-1H-benzimidazol-2-yl)-2-oxapropane]nickel(II) dipicrate-dimethylformamide-ethanol (1/2/0.25)
    Wu, Huilu
    Yun, Ruirui
    Li, Ke
    Wang, Kaitong
    Huang, Xingcai
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : M751 - U619
  • [3] Bis[1,3-bis(1-ethyl-1H-benzimidazol-2-yl)-2-oxapropane]cadmium(II) dipicrate dimethylformamide disolvate
    Wu, Huilu
    Liu, Bin
    Kou, Fan
    Jia, Fei
    Kong, Jin
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : M768 - U1182
  • [4] Bis[1,3-bis(1-propyl-1H-benzimidazol-2-yl)-2-oxapropane]cadmium(II) dipicrate dimethylformamide monosolvate
    Wu, Huilu
    Kou, Fan
    Jia, Fei
    Liu, Bin
    Yuan, Jingkun
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : M1461 - U1466
  • [5] Bis[1,3-bis(benzimidazol-2-yl)-2-oxapropane]cobalt(II) dipicrate acetonitrile trisolvate
    Wu, Huilu
    Yun, Ruirui
    Huang, Xingcai
    Sun, Qingyu
    Qi, Baoliang
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : M851 - U283
  • [6] 1,3-Bis(1-methyl-1H-benzimidazol-2-yl)-2-oxapropane
    Kou, Fan
    Liu, Bin
    Bai, Ying
    Kong, Jin
    Wu, Huilu
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1439 - U916
  • [7] Aqua[1,3-bis(benzimidazol-2-yl)-2oxapropane]diethanolmanganese(II) dipicrate ethanol disolvate
    Sun, Tao
    Li, Ke
    Lai, Yulin
    Chen, Ruihuan
    Wu, Huilu
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M1058 - U254
  • [8] Bis[1,3-bis(1-methyl-1H-benzimidazol-2-yl)-2-oxapropane]cadmium dipicrate acetonitrile sesquisolvate 0.25-hydrate
    Wu, Huilu
    Kou, Fan
    Jia, Fei
    Yuan, Jingkun
    Liu, Bin
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : M647 - U1290
  • [9] Bis[1,3-bis(benzimidazol-2-yl)-2-oxapropane]copper(II)-picrate-dimethyl-formamide (1/2/4)
    Yun, Ruirui
    Ying, Wei
    Qi, Baoliang
    Fan, Xuyang
    Wu, Huilu
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : M1529 - U469
  • [10] Bis[2,6-bis(1H-benzimidazol-2-yl)pyridine]nickel(II) dipicrate dimethylformamide disolvate
    Huang, Xingcai
    Kou, Fan
    Qi, Baoliang
    Meng, Xuan
    Wu, Huilu
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M967 - U983
12345