Synthesis of 4-(2-Hydroxy-5-methylphenyl)-1,3-Dithiol-2-ylidene Derivatives

被引:0
作者
Lungu, Catalin Neculai [1 ]
Asaftei, Iuliean Vasile [1 ]
Sandu, Ion [2 ,3 ]
Chirita, Paul [4 ]
Bahrin, Lucian Gabriel [1 ,5 ]
机构
[1] Alexandru Ioan Cuza Univ, Dept Chem, 11 Carol I Blvd, Iasi 700506, Romania
[2] Alexandru Ioan Cuza Univ, Arheoinvest Platform, Sci Invest Lab, 11 Carol I Blvd, Iasi 700506, Romania
[3] Romanian Inventors Forum, 3 Sf Petru Movila Str,Bloc L11,3-3, Iasi 700089, Romania
[4] Univ Craiova, Dept Chem, 1071 Calea Bucuresti, Craiova 200478, Romania
[5] Petru Poni Inst Macromol Chem, 41 A Grigore Ghica Voda Alley, Iasi 700487, Romania
来源
REVISTA DE CHIMIE | 2019年 / 70卷 / 05期
关键词
acetophenones; 1,3-dithiolium salts; methylene active; ylidenes; SELECTIVE SYNTHESIS; BRIDGE;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The reaction of 4-(2-hydroxy-5-methylphenyl)-1,3-dithiolium perchlorates with various methylene active compounds has provided the corresponding 1,3-dithiol-2-ylidene derivatives. The reactions have been performed under basic conditions using DBU. The newly obtained derivatives were characterized by NMR, MS spectrometry and IR spectroscopy.
引用
收藏
页码:1558 / 1560
页数:3
相关论文
共 25 条
  • [1] Novel 4-(3-Bromo-2-hydroxy-5-methylphenyl)-1,3-Dithiol-2-ylidene Derivatives
    Gorodea, Ioana Aurelia
    Sandu, Ion
    Sarbu, Laura Gabriela
    [J]. REVISTA DE CHIMIE, 2017, 68 (09): : 1988 - 1991
  • [2] 4-(2-Hydroxyphenyl)-1,3-Dithiol-2-ylidene Derivatives
    Lungu, Catalin Neculai
    Asaftei, Iuliean Vasile
    Sandu, Ion
    Bahrin, Lucian Gabriel
    [J]. REVISTA DE CHIMIE, 2019, 70 (01): : 161 - 164
  • [3] Synthesis of Novel 1,3-Dithiol-2-ylidene Derivatives from the Corresponding Mesoionic Compound
    Bahrin, Lucian Gabriel
    Craciun, Bogdan Florin
    Sandu, Ion
    Birsa, Mihail Lucian
    [J]. REVISTA DE CHIMIE, 2014, 65 (05): : 525 - 528
  • [4] The Synthesis and X-Ray Structural Characterization of New 4-(5-Bromo-2-hydroxyphenyl)-1,3-Dithiol-2-ylium Perchlorates
    Hrib, Cristian George
    Chirita, Paul
    Sandu, Ioan Gabriel
    Asaftei, Iuliean Vasile
    Sarbu, Laura Gabriela
    Earar, Kamel
    [J]. REVISTA DE CHIMIE, 2015, 66 (07): : 983 - 986
  • [5] Mesoionic 4-(2-Dialkylamino-1,3-dithiol-2-ylium-4-yl)phenolates
    Chirita, Paul
    Asaftei, Iuliean Vasile
    Sandu, Ion
    Sarbu, Laura Gabriela
    Lupu, Vasile Valeriu
    [J]. REVISTA DE CHIMIE, 2017, 68 (01): : 147 - 150
  • [6] 2-Alkylimino-4-(2-Hydroxyaryl)-1,3-Dithiols Derivatives
    Sarbu, Laura Gabriela
    Lungu, Catalin Neculai
    Sandu, Ion
    [J]. REVISTA DE CHIMIE, 2019, 70 (03): : 745 - 748
  • [7] 5-Methyl-4-(5-Bromo-2-hydroxyphenyl)-1,3-Dithiolium Derivatives
    Lungu, Catalin Neculai
    Sandu, Ion
    Sarbu, Laura Gabriela
    [J]. REVISTA DE CHIMIE, 2018, 69 (12): : 3549 - 3552
  • [8] Synthesis and Properties of 1,3-Dialkyl-4-nitro-1,2,3-triazolium Salts
    Sukhanov, G. T.
    Filippova, Yu, V
    Bagryanskaya, I. Yu
    Sukhanova, A. G.
    Bosov, K. K.
    Krupnova, I. A.
    Pivovarova, E., V
    [J]. CHEMISTRY FOR SUSTAINABLE DEVELOPMENT, 2021, 29 (06): : 684 - 689
  • [9] Efficient synthesis of novel cyclic fused-phenothiazines via domino cyclization of 2-(benzo[b][1,4]thiazin-3-ylidene)acetate, aromatic aldehydes and cyclic 1,3-diketones
    Sun, Jing
    Sun, Quan-Shun
    Yan, Chao-Guo
    [J]. ORGANIC CHEMISTRY FRONTIERS, 2019, 6 (20): : 3555 - 3561
  • [10] Synthesis of 2-phenyl pyridine derivatives from aryl ketones and 1,3-diaminopropane using palladium acetate as a catalyst
    Ghodse, Shrikant M.
    Telvekar, Vikas N.
    [J]. TETRAHEDRON LETTERS, 2017, 58 (06) : 524 - 526