Hydrothermal synthesis of nano ZrO2 powders

被引:12
作者
Duran, Cihangir
Yu, Jia
Sato, Kimiyasu
Hotta, Yuji
Watari, Koji
机构
[1] Natl Inst Adv Ind Sci & Technol, Adv Sintering Technol Grp, Adv Mfg Res Inst, Moriyama Ku, Nagoya, Aichi, Japan
[2] Gebze Inst Techol, Dept Mat Sci & Engn, TR-41400 Gebze, Turkey
来源
SCIENCE OF ENGINEERING CERAMICS III | 2006年 / 317-318卷
关键词
hydrothermal synthesis; nano powders; ZrO2;
D O I
10.4028/www.scientific.net/KEM.317-318.195
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Hydrothermal synthesis of nano ZrO2 powders were carried out at a temperature range of 100 to 200 degrees C, using zirconium solution. Formation of ZrO2 formation was accelerated with temperature and precipitation of ZrO2 took place directly from the solution. XRD analysis revealed that monoclinic ZrO2 was formed at all conditions. Crystallite size was found to range from 2.6 to 4 nm. Mean particle size increased from 93 nm at 135 degrees C to 125 nm at 200 degrees C after reaction time of 2 h.
引用
收藏
页码:195 / 198
页数:4
相关论文
共 7 条
[1]  
ADAIR JH, 1990, CERAM TRANS, V12, P25
[2]   A HYDROTHERMAL ROUTE FOR PRODUCTION OF DENSE, NANOSTRUCTURED Y-TZP [J].
BOUTZ, MMR ;
SCHOLTENHUIS, RJMO ;
WINNUBST, AJA ;
BURGGRAAF, AJ .
MATERIALS RESEARCH BULLETIN, 1994, 29 (01) :31-40
[3]  
Cheng HM, 1999, J EUR CERAM SOC, V19, P1675, DOI 10.1016/S0955-2219(98)00266-0
[4]   CHARACTERIZATION AND STABILIZATION OF METASTABLE TETRAGONAL ZRO2 [J].
MITSUHASHI, T ;
ICHIHARA, M ;
TATSUKE, U .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1974, 57 (02) :97-101
[5]   A STUDY ON PREPARATION OF TETRAGONAL ZIRCONIA POLYCRYSTALS (TZP) IN THE TIO2-Y2O3-ZRO2 SYSTEM [J].
PYDA, W ;
HABERKO, K ;
BUCKO, MM ;
FARYNA, M .
CERAMICS INTERNATIONAL, 1992, 18 (05) :321-326
[6]   FORMATION OF ULTRAFINE TETRAGONAL ZRO2 POWDER UNDER HYDROTHERMAL CONDITIONS [J].
TANI, E ;
YOSHIMURA, M ;
SOMIYA, S .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1983, 66 (01) :11-14
[7]   Hydrothermal synthesis of crystallized nano-particles of rare earth-doped zirconia and hafnia [J].
Yoshimura, M ;
Somiya, S .
MATERIALS CHEMISTRY AND PHYSICS, 1999, 61 (01) :1-8