The use of non-contact AFM with nanoindentation techniques for measuring mechanical properties of carbon nitride thin films

被引:17
作者
Chowdhury, S [1 ]
Laugier, MT [1 ]
机构
[1] Univ Limerick, Dept Phys, MSSI, Limerick, Ireland
关键词
AFM imaging; carbon nitride thin films; nanoindentation;
D O I
10.1016/j.apsusc.2004.03.255
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Non-contact AFM imaging was used to investigate the response of a material at small scales during nanoindentation. The true residual area measured from the AFM images can subsequently be used to recalculate the hardness of the material measured by nanoindentation more accurately. In this study, nanoindentation with non-contact AFM has been used to investigate the mechanical properties of thin CN films deposited by rf magnetron sputtering on silicon (100) substrates. Hardness was determined at different loads and depths from nanoindentation using the Oliver and Pharr method. The indents were imaged using AFM and true residual contact areas as well as hardness values were determined. Hardness values obtained by AFM agreed with the hardness measured by the Oliver and Pharr method. (C) 2004 Elsevier B.V. All rights reserved.
引用
收藏
页码:219 / 226
页数:8
相关论文
共 11 条
[1]   A nanoindentation study of copper films on oxidised silicon substrates [J].
Beegan, D ;
Chowdhury, S ;
Laugier, MT .
SURFACE & COATINGS TECHNOLOGY, 2003, 176 (01) :124-130
[2]   MICROSCOPY AND MICROINDENTATION MECHANICS OF SINGLE-CRYSTAL FE-3 WT-PERCENT-SI .1. ATOMIC-FORCE MICROSCOPY OF A SMALL INDENTATION [J].
HARVEY, S ;
HUANG, H ;
VENKATARAMAN, S ;
GERBERICH, WW .
JOURNAL OF MATERIALS RESEARCH, 1993, 8 (06) :1291-1299
[3]   Growth, structure, and mechanical properties of CNxHy films deposited by dc magnetron sputtering in N2/Ar/H2 discharges [J].
Hellgren, N ;
Johansson, MP ;
Hjörvarsson, B ;
Broitman, E ;
Östblom, M ;
Liedberg, B ;
Hultman, L ;
Sundgren, JE .
JOURNAL OF VACUUM SCIENCE & TECHNOLOGY A-VACUUM SURFACES AND FILMS, 2000, 18 (05) :2349-2358
[4]   On the hardness of coated systems [J].
Korsunsky, AM ;
McGurk, MR ;
Bull, SJ ;
Page, TF .
SURFACE & COATINGS TECHNOLOGY, 1998, 99 (1-2) :171-183
[5]   SIZE-DEPENDENT HARDNESS OF SILVER SINGLE-CRYSTALS [J].
MA, Q ;
CLARKE, DR .
JOURNAL OF MATERIALS RESEARCH, 1995, 10 (04) :853-863
[6]   Mechanical properties and characterisation of very thin CNx films synthesised by IBAD [J].
Malkow, T ;
Arce-García, I ;
Kolitsch, A ;
Schneider, D ;
Bull, SJ ;
Page, TF .
DIAMOND AND RELATED MATERIALS, 2001, 10 (12) :2199-2211
[7]  
OLIVER WC, 1992, J MATER RES, V7, P1562
[8]   APPLICATION OF ATOMIC-FORCE MICROSCOPY FOR MICROINDENTATION TESTING [J].
PETZOLD, M ;
LANDGRAF, J ;
FUTING, M ;
OLAF, JM .
THIN SOLID FILMS, 1995, 264 (02) :153-158
[9]   Measurement of mechanical properties by ultra-low load indentation [J].
Pharr, GM .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 1998, 253 (1-2) :151-159
[10]   NEW EVIDENCE FOR A PRESSURE-INDUCED PHASE-TRANSFORMATION DURING THE INDENTATION OF SILICON [J].
PHARR, GM ;
OLIVER, WC ;
HARDING, DS .
JOURNAL OF MATERIALS RESEARCH, 1991, 6 (06) :1129-1130