Electrochemical synthesis and structure characterization of nickel sulfide nanoparticles

被引：44
作者：
Fazli, Yousef [1 ]
Pourmortazavi, Seied Mahdi [2 ]
Kohsari, Iraj [3 ]
Sadeghpur, Meisam [2 ]
机构：
[1] Islamic Azad Univ, Fac Sci, Dept Chem, Arak Branch, Arak, Iran
[2] Malek Ashtar Univ Technol, Fac Mat & Mfg Technol, Tehran, Iran
[3] Amirkabir Univ Technol, Dept Chem, Tehran, Iran
来源：
MATERIALS SCIENCE IN SEMICONDUCTOR PROCESSING | 2014年 / 27卷
关键词：
Nanoparticle preparation; Nickel sulfide; Electrochemical synthesis; Statistical optimization; Taguchi robust design; ORTHOGONAL ARRAY DESIGN; SELECTIVE SYNTHESIS; OPTIMIZATION; NANOCRYSTALS; PARAMETERS; OXALATE;
D O I：
10.1016/j.mssp.2014.07.013
中图分类号：
TM [电工技术]; TN [电子技术、通信技术];
学科分类号：
0808 ; 0809 ;
摘要：
Nickel sulfide (NiS) nanoparticles were synthesized by a simple electrochemical route. In this study, synthesis conditions of nickel sulfide nanoparticles were optimized by Taguchi robust design. The current application of the Taguchi method was successful in optimizing the experimental parameters of the electrochemical synthesis procedure of nickel sulfide nano particles, The effects of several main procedure factors (i.e., sulfide ion concentration, applied voltage, stirring rate and reactor temperature) on the particle size of synthesized nickel sulfide particles were investigated. The significance of these factors on the diameter of nickel sulfide particles was evaluated by the analysis of variance (ANOVA) and the optimum conditions for the preparation of nickel sulfide rianoparticles by the proposed electrochemical method was proposed. The prepared NiS nanoparticles at optimum conditions were characterized by various techniques i.e., SEM, TEM, XRD, EDX, FT-IR, UV-vis and PL. (C) 2014 Elsevier Ltd. All rights reserved.
引用
收藏
页码：362 / 367
页数：6
相关论文
共 32 条
  • [1] Selective synthesis of Ni3S4 nanocrystallites with hollow structures through a solution-phase approach
    An, Changhua
    Zhang, Zhongjie
    Chen, Xiangying
    Liu, Yunqi
    [J]. MATERIALS LETTERS, 2006, 60 (29-30) : 3631 - 3634
  • [2] Bhuiyan N.H., 1976, BANGLADESH J SCI IND, V11, P29
  • [3] New Surface-Directed Vapour Transport Methods for the Controlled Growth of Nickel Sulfide Nanomaterials
    Denholme, Saleem J.
    Gallagher, Jamie B.
    Dobson, Phillip S.
    Weaver, John M. R.
    Gregory, Duncan H.
    [J]. ISRAEL JOURNAL OF CHEMISTRY, 2010, 50 (04) : 515 - 523
  • [4] Synthesis and characterization of cobalt sulfide nanocrystals in the presence of thioglycolic acid via a simple hydrothermal method
    Emadi, Hamid
    Salavati-Niasari, Masoud
    Davar, Fatemeh
    [J]. POLYHEDRON, 2012, 31 (01) : 438 - 442
  • [5] Grau J, 1997, J AM CERAM SOC, V80, P941, DOI 10.1111/j.1151-2916.1997.tb02925.x
  • [6] Orthogonal array design for the optimization of silver recovery from waste photographic paper
    Hosseini, SG
    Pourmortazavi, SM
    Fathollahi, M
    [J]. SEPARATION SCIENCE AND TECHNOLOGY, 2004, 39 (08) : 1953 - 1966
  • [7] Optimization of plasma arc welding parameters by using the Taguchi method with the grey relational analysis
    Hsiao, Y. F.
    Tarng, Y. S.
    Huang, W. J.
    [J]. MATERIALS AND MANUFACTURING PROCESSES, 2008, 23 (01) : 51 - 58
  • [8] The composition of nanoparticulate nickel sulfide
    Huang, Shanshan
    Lopez-Cape, Elisa
    Manning, David A. C.
    Rickard, David
    [J]. CHEMICAL GEOLOGY, 2010, 277 (3-4) : 207 - 213
  • [9] Synthesis of nano-sized particles from metal carbonates by the method of reversed mycelles
    Karagiozov, C
    Montchilova, D
    [J]. CHEMICAL ENGINEERING AND PROCESSING-PROCESS INTENSIFICATION, 2005, 44 (01) : 115 - 119
  • [10] Synthesis of NiS nanoparticles using a sugar-ester nonionic water-in-oil microemulsion
    Khiew, PS
    Huang, NM
    Radiman, S
    Ahmad, MS
    [J]. MATERIALS LETTERS, 2004, 58 (05) : 762 - 767
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