Teaching UV Vis Spectroscopy with a 3D-Printable Smartphone Spectrophotometer

被引:129
作者
Grasse, Elise K. [1 ]
Torcasio, Morgan H. [1 ]
Smith, Adam W. [1 ]
机构
[1] Univ Akron, Dept Chem, 190 Buchtel Common, Akron, OH 44325 USA
关键词
Laboratory Instruction; High School/Introductory Chemistry; Upper-Division Undergraduate; Analytical Chemistry; Hands-On Learning/Manipulatives; UV-Vis Spectroscopy; Problem Solving/Decision Making; Calibration; Dyes/Pigments; IMMUNOSORBENT-ASSAY ELISA; COLORIMETER; ABSORPTION;
D O I
10.1021/acs.jchemed.5b00654
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Visible absorbance spectroscopy is a widely used tool in chemical, biochemical, and medical laboratories. The theory and methods of absorbance spectroscopy are typically introduced in upper division undergraduate chemistry courses, but could be introduced earlier with the right curriculum and instrumentation. A major challenge in teaching spectroscopy is gaining access to laboratory equipment, which can be expensive. Even common educational spectrophotometers still carry a substantial cost and have the disadvantage of being inherently closed designs. We report on a 3D-printable smartphone spectrophotometer that is very inexpensive to build, yet retains the functionality and analytical accuracy necessary to teach concepts like the Beer Lambert Law. The optical components are arranged in an intuitive, accessible way so that students can see each relevant part and experiment with the parameters. Here, we describe the device and provide exercises to teach different concepts in analytical spectrophotometry.
引用
收藏
页码:146 / 151
页数:6
相关论文
共 24 条
[1]   Open-Source Colorimeter [J].
Anzalone, Gerald C. ;
Glover, Alexandra G. ;
Pearce, Joshua M. .
SENSORS, 2013, 13 (04) :5338-5346
[2]   A SIMPLE MICROWELL COLORIMETER FOR USE IN AN INTRODUCTORY CHEMISTRY LAB [J].
CRUMP, J ;
SANDWICK, RK .
JOURNAL OF CHEMICAL EDUCATION, 1994, 71 (08) :A199-A200
[3]   ENZYME-LINKED IMMUNOSORBENT ASSAY (ELISA) QUANTITATIVE ASSAY OF IMMUNOGLOBULIN-G [J].
ENGVALL, E ;
PERLMANN, P .
IMMUNOCHEMISTRY, 1971, 8 (09) :871-&
[4]   A LED microtiter plate reader [J].
Gordon, J ;
Tye, S .
JOURNAL OF CHEMICAL EDUCATION, 2005, 82 (06) :903-905
[5]   A graduated cylinder colorimeter: An investigation of path length and the Beer-Lambert law [J].
Gordon, J ;
Harman, S .
JOURNAL OF CHEMICAL EDUCATION, 2002, 79 (05) :611-612
[6]   Development of a low-cost four-color LED photometer [J].
Hamilton, JR ;
White, JS ;
Nakhleh, MB .
JOURNAL OF CHEMICAL EDUCATION, 1996, 73 (11) :1052-1054
[7]   Crime Scene Investigation in the Art World: The Case of the Missing Masterpiece [J].
Harmon, Katharine J. ;
Miller, Lisa M. ;
Millard, Julie T. .
JOURNAL OF CHEMICAL EDUCATION, 2009, 86 (07) :817-819
[8]   Combined "dual" absorption and fluorescence smartphone spectrometers [J].
Hossain, Md. Arafat ;
Canning, John ;
Ast, Sandra ;
Cook, Kevin ;
Rutledge, Peter J. ;
Jamalipour, Abbas .
OPTICS LETTERS, 2015, 40 (08) :1737-1740
[9]   A LOW-COST PRECISION COLORIMETER [J].
JAFFAR, M ;
ZAHID, Q .
JOURNAL OF CHEMICAL EDUCATION, 1988, 65 (12) :1099-1100
[10]   An educational spectrograph using a digital camera as a training aid for physics students [J].
Kiisk, V. .
EUROPEAN JOURNAL OF PHYSICS, 2014, 35 (03)