Novel dendritic cores based on thiacalix[4]arene derivatives

被引：25
|
作者：
Appelhans, D
Stastny, V
Komber, H
Voigt, D
Voit, B
Lhoták, P
Stibor, I
机构：
[1] Inst Polymer Res Dresden, Dresden, Germany
[2] Inst Chem Technol, Dept Organ Chem, Prague 16628 6, Czech Republic
来源：
TETRAHEDRON LETTERS | 2004年 / 45卷 / 38期
关键词：
thiacalixarenes; benzylic spacer; dendritic core; amino surface group;
D O I：
10.1016/j.tetlet.2004.07.085
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Thiacalix[4]arenes possessing carboxylic groups were used for the design of potential dendritic cores with amino surface groups. The known tetraacetic acid in the 1,3-alternate conformation gave the desired product in very low yield because of steric hindrance on thiacalix[4]arene moiety. Therefore, synthetic strategy based on withdrawing of the carboxyl groups via benzylic spacer from the thiacalix[4]arene moiety was successfully applied for the realization of novel thiacalix[4]arenes bearing two or four protected lysine units. (C) 2004 Elsevier Ltd. All rights reserved.
引用
收藏
页码：7145 / 7149
页数：5
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