KF-silica as a stationary phase for the chromatographic removal of tin residues from organic compounds

被引:80
作者
Harrowven, DC [1 ]
Guy, IL [1 ]
机构
[1] Univ Southampton, Dept Chem, Southampton SO17 1BJ, Hants, England
关键词
D O I
10.1039/b406041e
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Through the simple expedient of using a mixture of KF and silica as the stationary phase in column chromatography, levels of organotin impurities from tributyltin hydride mediated reductions have been reduced from stoichiometric levels to similar to30 ppm.
引用
收藏
页码:1968 / 1969
页数:2
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