(E)-N′-(3,4-Dimethoxybenzylidene)-2,4-dihydroxybenzohydrazide methanol solvate

被引:1
作者
Zhang, Qiao-Ling [1 ]
Yin, Zi [1 ]
Deng, Xu-Ming [1 ]
Liu, Song-Cai [1 ]
Song, De-Guang [1 ]
机构
[1] Jilin Univ, Coll Anim Sci & Vet Med, Changchun 130062, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷
关键词
BIOLOGICAL-ACTIVITY; HYDRAZIDE;
D O I
10.1107/S1600536809035752
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C(16)H(16)N(2)O(5)center dot CH(3)OH, was obtained from a condensation reaction of 3,4-dimethoxybenzaldehyde and 2,4-dihydroxybenzohydrazide. The non-H atoms of the Schiff base molecule are approximately coplanar (r.m.s. deviation = 0.043 angstrom) and the dihedral angle between the two benzene rings is 1.6 (1)degrees. The molecule adopts an E configuration with respect to the C=N double bond. An intramolecular O-H center dot center dot center dot O hydrogen bond is observed. The Schiff base and methanol molecules are linked into a two-dimensional network parallel to (10 (1) over bar) by intermolecular N-H center dot center dot center dot O, O-H center dot center dot center dot N and O-H center dot center dot center dot O hydrogen bonds.
引用
收藏
页码:O2392 / +
页数:10
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