Multiple dual-mode centrifugal partition chromatography as an efficient method for the purification of a mycosporine from a crude methanolic extract of Lichina pygmaea

被引：40

作者：

Roullier, Catherine ^{[1
]}

Chollet-Krugler, Marylene ^{[1
]}

Bernard, Aurelie ^{[1
]}

Boustie, Joel ^{[1
]}

机构：

[1] Univ Rennes 1, EA Subst Lichen & Photoprotect 4090, UFR Sci Pharmaceut & Biol, Univ Europeenne Bretagne, F-35043 Rennes, France

来源：

JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES | 2009年 / 877卷 / 22期

关键词：

Centrifugal partition chromatography; Multiple-dual-mode; Lichina pygmaea; Purification; Isolation; Mycosporine; AMINO-ACIDS; ABSORBING MYCOSPORINE; UV; COMPOUND;

D O I：

10.1016/j.jchromb.2009.05.040

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

Centrifugal partition chromatography method was applied to the separation and purification of a crude methanolic extract of a cyanobacterial lichen, Lichina pygmaea. A multiple dual-mode was used to separate two compounds of interest, namely mycosporine-serinol and a glutamic acid derivative. These compounds are described here for the first time in a lichen. Their structures were identified by UV, IR, ESI-MS. H-1 NMIR, C-13 NMR, and 2D NMR. (C) 2009 Elsevier B.V. All rights reserved.

引用

页码：2067 / 2073

页数：7

共 11 条

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