Controlled synthesis of Pd-Pt alloy nanohypercubes under microwave irradiation

被引：18

作者：

Dai, Lei ^{[1
,2
]}

Zhao, Yanxi ^{[1
,2
]}

Chi, Quan ^{[1
,2
]}

Huang, Tao ^{[1
,2
]}

Liu, Hanfan ^{[1
,2
,3
]}

机构：

[1] South Cent Univ Nationalities, Coll Chem & Mat Sci, State Ethn Affairs Commiss, Key Lab Catalysis & Mat Sci, Wuhan 430074, Peoples R China

[2] South Cent Univ Nationalities, Coll Chem & Mat Sci, Minist Educ, Wuhan 430074, Peoples R China

[3] Chinese Acad Sci, Inst Chem, Beijing 100080, Peoples R China

来源：

CRYSTENGCOMM | 2014年 / 16卷 / 24期

关键词：

HIGH-INDEX FACETS; SHAPE-CONTROLLED SYNTHESIS; PALLADIUM NANOCRYSTALS; CATALYTIC-PROPERTIES; CONCAVE NANOCUBES; ELECTROCATALYTIC ACTIVITIES; METALLIC NANOSTRUCTURES; PLATINUM NANOCRYSTALS; HOLLOW NANOSTRUCTURES; ASSISTED SYNTHESIS;

D O I：

10.1039/c4ce00284a

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Pd-Pt alloy hypercubic nanostructures were successfully fabricated by reducing Pd and Pt precursors simultaneously in a one step process under microwave irradiation for only 100 s without using any sacrificial templates. Together with the use of tetraethylene glycol (TEG) as both a solvent and a reducing agent, the presence of KI was critical to the formation of Pd-Pt alloy nanohypercubes. The as-prepared Pd-Pt alloy nanohypercubes improved the electrocatalytic activities.

引用

页码：5206 / 5211

页数：6

共 50 条

[11]

Hayes BL, 2004, ALDRICHIM ACTA, V37, P66

[12] Controlled Synthesis of Pd-Pt Alloy Hollow Nanostructures with Enhanced Catalytic Activities for Oxygen Reduction [J].

Hong, Jong Wook ;

Kang, Shin Wook ;

Choi, Bu-Seo ;

Kim, Dongheun ;

Lee, Sang Bok ;

Han, Sang Woo .

ACS NANO, 2012, 6 (03) :2410-2419

[13] One-pot synthesis and electrocatalytic activity of octapodal Au-Pd nanoparticles [J].

Hong, Jong Wook ;

Lee, Young Wook ;

Kim, Minjung ;

Kang, Shin Wook ;

Han, Sang Woo .

CHEMICAL COMMUNICATIONS, 2011, 47 (09) :2553-2555

[14] Single-Crystalline Octahedral Au-Ag Nanoframes [J].

Hong, Xun ;

Wang, Dingsheng ;

Cai, Shuangfei ;

Rong, Hongpan ;

Li, Yadong .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2012, 134 (44) :18165-18168

[15] Amine-Assisted Synthesis of Concave Polyhedral Platinum Nanocrystals Having {411} High-Index Facets [J].

Huang, Xiaoqing ;

Zhao, Zipeng ;

Fan, Jingmin ;

Tan, Yueming ;

Zheng, Nanfeng .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2011, 133 (13) :4718-4721

[16]

Huang XQ, 2011, NAT NANOTECHNOL, V6, P28, DOI [10.1038/nnano.2010.235, 10.1038/NNANO.2010.235]

[17] Controlled Formation of Concave Tetrahedral/Trigonal Bipyramidal Palladium Nanocrystals [J].

Huang, Xiaoqing ;

Tang, Shaoheng ;

Zhang, Huihui ;

Zhou, Zhiyou ;

Zheng, Nanfeng .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2009, 131 (39) :13916-+

[18] Simplifying the Creation of Hollow Metallic Nanostructures: One-Pot Synthesis of Hollow Palladium/Platinum Single-Crystalline Nanocubes [J].

Huang, Xiaoqing ;

Zhang, Huihui ;

Guo, Changyou ;

Zhou, Zhiyou ;

Zheng, Nanfeng .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2009, 48 (26) :4808-4812

[19] One-Pot, High-Yield Synthesis of 5-Fold Twinned Pd Nanowires and Nanorods [J].

Huang, Xiaoqing ;

Zheng, Nanfeng .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2009, 131 (13) :4602-+

[20] Copper Can Still Be Epitaxially Deposited on Palladium Nanocrystals To Generate Core-Shell Nanocubes Despite Their Large Lattice Mismatch [J].

Jin, Mingshang ;

Zhang, Hui ;

Wang, Jinguo ;

Zhong, Xiaolan ;

Lu, Ning ;

Li, Zhiyuan ;

Xie, Zhaoxiong ;

Kim, Moon J. ;

Xia, Younan .

ACS NANO, 2012, 6 (03) :2566-2573

← 1 2 3 4 5 →