207Pb chemical shift thermometer at high temperature for magic angle spinning experiments

被引：117

作者：

Takahashi, T ^{[1
]}

Kawashima, H

Sugisawa, H

Baba, T

机构：

[1] Japan Energy Analyt Res Ctr, Toda, Saitama 335, Japan

[2] JEOL, Analyt Instrument Div, Akishima, Tokyo 196, Japan

[3] Tokyo Inst Technol, Dept Chem Engn, Meguro Ku, Tokyo 1528552, Japan

来源：

SOLID STATE NUCLEAR MAGNETIC RESONANCE | 1999年 / 15卷 / 02期

关键词：

temperature calibration; Pb-207 MAS NMR; high temperature;

D O I：

10.1016/S0926-2040(99)00039-9

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

The temperature dependence of Pb-207 chemical shift in magic angle spinning (MAS) NMR spectrum of Pb(NO3)(2) provides a sensitive method to calibrate sample temperatures in MAS NMR. The temperature dependence is uniform in the temperature range between 30 degrees C and 400 degrees C. The NMR sensitivity and the line width are also favorable. (C) 1999 Elsevier Science B.V. All rights reserved.

引用

页码：119 / 123

页数：5

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