Hydrothermal synthesis of nanocrystalline MxZn1-xFe2O4 (M = Ni, Mn, Co; x=0.40-0.60) powders

被引：41

作者：

Jiao, XL ^{[1
]}

Chen, DR ^{[1
]}

Hu, Y ^{[1
]}

机构：

[1] Shandong Univ, Dept Chem, Jinan 250100, Peoples R China

来源：

MATERIALS RESEARCH BULLETIN | 2002年 / 37卷 / 09期

关键词：

magnetic materials; oxides; chemical synthesis; X-ray diffraction;

D O I：

10.1016/S0025-5408(02)00857-7

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

A series of nanocrystalline MxZn1-xFe2O4 (M = Ni, Mn and Co; x = 0.40-0.60) powders have been successfully prepared via hydrothermal process and characterized by XRD, TEM and IR techniques. The effects of reaction temperature and the initial pH value of the starting suspension solution on the particulate properties such as the particle size and morphology are discussed. IR spectra indicate that there are no hydroxyl in as-prepared NixZn1-xFe2O4 and CoxZn1-xFe2O4 powders, while there are obvious hydroxyl adsorption on the IR spectrum of MnxZn1-xFe2O4 powder. (C) 2002 Elsevier Science Ltd. All rights reserved.

引用

页码：1583 / 1588

页数：6

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