Supramolecular motifs in metal complexes of malonic acid dihydrazide: copper(II) and zinc(II) assisted assembly of malonic acid dihydrazide with melamine

被引：1
|
作者：
Mishra, L
Pathak, B
Agrawal, Y [1 ]
机构：
[1] Gujarat Univ, Dept Chem, Ahmadabad 380009, Gujarat, India
[2] Banaras Hindu Univ, Dept Chem, Varanasi 221005, Uttar Pradesh, India
来源：
TRANSITION METAL CHEMISTRY | 2004年 / 29卷 / 04期
关键词：
D O I：
10.1023/B:TMCH.0000027456.94456.b3
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
One pot condensation of malonic acid dihydrazide (MADH) in the presence of metal salts (CuCl2 . H2O and ZnCl2) with melamine (TAT) has been achieved. The solids Cu(MADH)(2)Cl-2 . 2TAT . 9H(2)O and Zn(MADH)(2)Cl-2 . TAT . 1/2H(2)O thus obtained were characterized by elemental analysis, FAB mass, i.r., n.m.r., u.v.-visible and e.p.r. spectral data together with their powder X-ray diffraction, optical microscopy, scanning electron microscopy (SEM) and atomic force microscopy (AFM) ( Zn complex only). Variable temperature solid slate conductance measurements have also been made.
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页码：437 / 443
页数：7
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