Preparation and fluorescence property of pure Bi2SiO5 powders by Pechini sol-gel method

被引：10
|
作者：
Wu, Yuanting [1 ]
Li, Menglong [1 ]
Wang, Xiufeng [1 ]
Wang, Lili [1 ]
Gao, Hui [1 ]
机构：
[1] Shaanxi Univ Sci & Technol, Sch Mat Sci & Engn, Xian 710021, Peoples R China
来源：
MATERIALS AND MANUFACTURING PROCESSES | 2017年 / 32卷 / 05期
基金：
中国国家自然科学基金;
关键词：
Gel; low-temperature; optics; particles; phase; powder; synthesis; XRD; BISMUTH SILICATE; TITANIUM; FILMS;
D O I：
10.1080/10426914.2016.1221081
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Metastable Bi2SiO5 phase powders were synthesized successfully by Pechini sol-gel method using a simple starting hydro-alcoholic solution consisting of Bi(NO3)(3)<bold></bold>5H(2)O, TEOS, citric acid, and PEG-6000. The effects of Bi/Si molar ratio, citric acid, and PEG-6000 on the properties of pure Bi2SiO5 powders were investigated. The crystalline phase and fluorescence properties were characterized. The process of Pechini sol-gel method and the effect of purity on fluorescence properties were studied in this paper. X-ray diffraction results illustrate that single phase of Bi2SiO5 can be obtained at 650 degrees C for 1h. Furthermore, the maximum fluorescence emission wavelength of the powders is located at 355 nm, which represents the band gap of Bi2SiO5 powders is 3.49 eV.
引用
收藏
页码：480 / 483
页数：4
相关论文
共 50 条
  • [1] Low temperature synthesis and photocatalytic performances of pure Bi2SiO5 powders via pechini sol-gel method
    Wu, Yuanting
    Li, Menglong
    Yuan, Jun
    Wang, Xiufeng
    JOURNAL OF MATERIALS SCIENCE-MATERIALS IN ELECTRONICS, 2017, 28 (14) : 10406 - 10410
  • [2] Low temperature synthesis and photocatalytic performances of pure Bi2SiO5 powders via pechini sol–gel method
    Yuanting Wu
    Menglong Li
    Jun Yuan
    Xiufeng Wang
    Journal of Materials Science: Materials in Electronics, 2017, 28 : 10406 - 10410
  • [3] A novel method for preparation of pure Bi2SiO5 crystals
    Guo, H. W.
    Wang, X. F.
    Gao, D. N.
    MATERIALS LETTERS, 2012, 67 (01) : 280 - 282
  • [4] Preparation of Bi2SiO5 metastable phase powders by chemical solution decomposition method
    Xu, Ya-Qin
    Wang, Xiu-Feng
    Jiang, Hong-Tao
    Lu, Jun-Que
    Rengong Jingti Xuebao/Journal of Synthetic Crystals, 2011, 40 (06): : 1541 - 1546
  • [5] SiO2 Powders Synthesized via Sol-gel as Pure Raw Material in Geopolymer Preparation
    Dell'Aversano, Raffaella
    Fontana, Elisabetta
    Barrino, Federico
    Catauro, Michelina
    9TH INTERNATIONAL CONFERENCE ON STRUCTURAL ANALYSIS OF ADVANCED MATERIALS (ICSAAM 2019), 2019, 2196
  • [6] PREPARATION AND PROPERTIES OF PURE NANOCOMPOSITE FE-SIO2 USING THE SOL-GEL METHOD
    WANG, JP
    LUO, HL
    JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 1994, 131 (1-2) : 54 - 60
  • [7] Preparation of porous SiO2 ultrafine powders by sol-gel process
    Zhongnan Gongye Daxue Xuebao, 2 (131-134):
  • [8] Preparation of amorphous Al2O3-2SiO2 powders with alkali-activation property by sol-gel method
    Zheng Guangjian
    Cui Xuemin
    Zhang Weipeng
    Tong Zhangfa
    RARE METAL MATERIALS AND ENGINEERING, 2007, 36 : 137 - 139
  • [9] Preparation and Magnetic Property of Co-Doped ZnO Powders by Sol-Gel Method
    Zhou Xuan
    Wang Chuanbin
    Luo Sijun
    Shen Qiang
    Zhang Lianmeng
    RARE METAL MATERIALS AND ENGINEERING, 2013, 42 : 212 - 214
  • [10] Preparation and Characterization of Barium Titanate (BaTiO3) Nano-Powders by Pechini Sol-Gel Method
    Wu, Yuan Ting
    Wang, Xiu Feng
    Yu, Cheng Long
    Li, Er Yuan
    MATERIALS AND MANUFACTURING PROCESSES, 2012, 27 (12) : 1329 - 1333
12345