Synthesis and characterization of mesoporous MCM-41 templated by the mixture of cationic-anionic surfactant

被引：0
|
作者：
Tai, Xiumei [1 ]
Wong, Hongxia [1 ]
Du, Zhiping [1 ]
Shi, Xiuqi [1 ]
机构：
[1] China Res Inst Daily Chem Ind, Taiyuan 030001, Shanxi Province, Peoples R China
来源：
TENSIDE SURFACTANTS DETERGENTS | 2006年 / 43卷 / 02期
关键词：
MCM-41; template; cationic-anionic surfactant; room temperature; synthesis;
D O I：
10.3139/113.100291
中图分类号：
O69 [应用化学];
学科分类号：
081704 ;
摘要：
Using the mixture of cationic cetyltrimethylammonium bromide (CTAB) and anionic Sodium Alkyl Epoxy Ethylene Carboxylate (AEC(9)Na) as template, tetraethyl orthosilicate (TEOS) as silica source, ethylenediamine (EDA) as base source, mesoporous MCM-41 has been synthesized at room temperature, characterized by X-ray power diffraction (XRD) and N-2 adsorption. The results showed that with the change of the ratio of cationic to anionic surfactant the pore size can be controlled and the mesoporous MCM-41 has larger pore size than that synthesized by using CTAB alone as template.
引用
收藏
页码：103 / 105
页数：3
相关论文
共 50 条
  • [21] Synthesis and characterization of the mesoporous galloaluminosilicate molecular sieve MCM-41
    Cheng, CF
    Klinowski, J
    JOURNAL OF THE CHEMICAL SOCIETY-FARADAY TRANSACTIONS, 1996, 92 (02): : 289 - 292
  • [22] THE ROLE OF SURFACTANT MICELLES IN THE SYNTHESIS OF THE MESOPOROUS MOLECULAR-SIEVE MCM-41
    CHENG, CF
    LUAN, ZH
    KLINOWSKI, J
    LANGMUIR, 1995, 11 (07) : 2815 - 2819
  • [23] Synthesis of high-quality mesoporous MCM-41 templated CTAB in nonaqueous system
    Lei, L
    Gao, YZ
    Jin, XD
    TENSIDE SURFACTANTS DETERGENTS, 2004, 41 (01) : 7 - 9
  • [24] Preparation and characterization of mesoporous MCM-41 membrane
    Chi, Cai-Xia
    Wei, Chang-Ping
    Jiang, Xiao-Guang
    Zhejiang Daxue Xuebao (Gongxue Ban)/Journal of Zhejiang University (Engineering Science), 2008, 42 (03): : 498 - 501
  • [25] THE PREPARATION AND CHARACTERIZATION OF MESOPOROUS ALUMINOSILICATES (MCM-41)
    FENG, XB
    HALLER, GL
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1994, 207 : 130 - COLL
  • [26] More economical synthesis of mesoporous MCM-41
    Kawi, S
    Lai, WW
    CHEMTECH, 1998, 28 (12) : 26 - 30
  • [27] SYNTHESIS OF FUNCTIONALIZED MCM-41 MESOPOROUS SILICA
    Mermer, Nevin Karamahmut
    Yilmaz, Muge Sari
    CBU INTERNATIONAL CONFERENCE PROCEEDINGS 2017: INNOVATIONS IN SCIENCE AND EDUCATION, 2017, 5 : 1164 - 1168
  • [28] Synthesis of MCM-41 mesoporous molecular sieves
    Franke, O
    Rathousky, J
    SchulzEkloff, G
    Zukal, A
    PREPARATION OF CATALYSTS VI: SCIENTIFIC BASES FOR THE PREPARATION OF HETEROGENEOUS CATALYSTS, 1995, 91 : 309 - 318
  • [29] Preparation of MCM-41 silica using the cationic surfactant blend
    Zukal, Arnost
    Siklova, Helena
    Cejka, Jiri
    Thommes, Matthias
    ADSORPTION-JOURNAL OF THE INTERNATIONAL ADSORPTION SOCIETY, 2007, 13 (3-4): : 247 - 256
  • [30] Synthesis and characterization of TiOxNy assembled in oxynitrided mesoporous silica MCM-41
    Zheng, S
    Li, ZP
    Gao, L
    MATERIALS CHEMISTRY AND PHYSICS, 2004, 85 (01) : 195 - 200
12345