Sonoelectrochemical Synthesis of Metallic Aluminum Nanoparticles

被引:40
作者
Mahendiran, Chinnathambi [1 ]
Ganesan, Raman [1 ]
Gedanken, Aharon [1 ]
机构
[1] Bar Ilan Univ, Dept Chem, Kanbar Lab Nanomat, Inst Nanotechnol & Adv Mat, IL-52900 Ramat Gan, Israel
关键词
Electrochemistry; Aluminum; Nanoparticles; TIME;
D O I
10.1002/ejic.200900097
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
In this paper, we report for the first time on the room-temperature preparation of metallic aluminum nanoparticles by the pulsed sonoelectrochemical method. The prepared nanoparticles were characterized by X-ray diffraction (XRD), high-resolution scanning electron microscopy, transmission electron microscopy (TEM), and high-resolution transmission electron microscopy. TEM analysis shows that the prepared aluminum nanoparticles range from 10 to 20 nm in size. The XRD pattern confirms the formation of metallic aluminum nanoparticles. The results show that the sonoelectrochemical technique is a promising method for the fabrication of air-sensitive metallic nanoparticles that have a high, negative reduction potential. ((C) Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2009)
引用
收藏
页码:2050 / 2053
页数:4
相关论文
共 26 条
[1]   Macroporous materials - electrochemically grown photonic crystals [J].
Braun, PV ;
Wiltzius, P .
CURRENT OPINION IN COLLOID & INTERFACE SCIENCE, 2002, 7 (1-2) :116-123
[2]   Thinking big (and small) about energetic materials [J].
Dlott, DD .
MATERIALS SCIENCE AND TECHNOLOGY, 2006, 22 (04) :463-473
[3]   Electrodeposition of nano- and microcrystalline aluminium in three different air and water stable ionic liquids [J].
El Abedin, S. Zein ;
Moustafa, E. M. ;
Hempelmann, R. ;
Natter, H. ;
Endres, F. .
CHEMPHYSCHEM, 2006, 7 (07) :1535-1543
[4]  
Fan Z. Y., 2007, P SPIE C, V6479
[5]   Influence of the microstructure of aluminium alloys on their residual impact properties after a fatigue loading program [J].
Froustey, Catherine ;
Lataillade, Jean Luc .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2009, 500 (1-2) :155-163
[6]   Pulsed sonoelectrochemical synthesis of polyaniline nanoparticles and their capacitance properties [J].
Ganesan, Raman ;
Shanmugam, Sangaraju ;
Gedanken, Aharon .
SYNTHETIC METALS, 2008, 158 (21-24) :848-853
[7]   Grain boundary sliding during friction stir spot welding of an aluminum alloy [J].
Gerlich, A. P. ;
Shibayanagi, T. .
SCRIPTA MATERIALIA, 2009, 60 (04) :236-239
[8]   Sonoelectrochemistry of Cu2+ in the presence of cetyltrimethylammonium bromide:: Obtaining CuBr instead of copper [J].
Haas, I ;
Gedanken, A .
CHEMISTRY OF MATERIALS, 2006, 18 (05) :1184-1189
[9]   Synthesis of metallic magnesium nanoparticles by sonoelectrochemistry [J].
Haas, Iris ;
Gedanken, Aharon .
CHEMICAL COMMUNICATIONS, 2008, (15) :1795-1797
[10]   Pulsed sonoelectrochemical synthesis of size-controlled copper nanoparticles stabilized by poly(n-vinylpyrrolidone) [J].
Haas, Iris ;
Shanmugam, Sangaraju ;
Gedanken, Aharon .
JOURNAL OF PHYSICAL CHEMISTRY B, 2006, 110 (34) :16947-16952