Fat extraction from fleshings - optimization of operating conditions

被引:7
作者
Cunha, A. F. [1 ]
Caetano, N. S. [1 ]
Ramalho, E. [1 ]
Crispim, A. [1 ]
机构
[1] IPP ISEP, CIETI ISEP Ctr Innovat Engn & Ind Technol, Sch Engn, R Dr Antonio Bernardino de Almeida 431, P-4249015 Porto, Portugal
关键词
Biowaste; Fat extraction; Fleshings; Hydrolysis; Tannery waste; BIODIESEL PRODUCTION; DIESEL; FEEDSTOCK; OILS;
D O I
10.1016/j.egyr.2020.11.176
中图分类号
TE [石油、天然气工业]; TK [能源与动力工程];
学科分类号
0807 ; 0820 ;
摘要
Fat from fleshings is an excellent source of energy since it is composed of glycerides, fatty acids and glycerol. The present work aims to optimize the operating conditions of fat extraction from fleshings. Animal fat was obtained after thermal treatment of fleshings in a stainless steel batch reactor using different operating conditions (100 <= T <= 155 degrees C; 1 <= P <= 5.5 bar, t= 2 h, r= 1000 rpm). The fat containing phases were extracted in a heated Soxhlet using n-hexane and ethanol to recover the fat from the solid residue. In addition, 6 M HCl acid was added to the remaining solid and heated to boiling conditions for 2 h to further extract fat that is encapsulated in the tissues of the fleshing. The best conditions of fat extraction were obtained at 155 degrees C during 2 h and 1000 rpm that generated a pressure of 5.5 bar inside the batch reactor. It was also found that significantly higher amount of fat could be obtained at the operating conditions mentioned (similar to 50 wt. % on dry basis), sparring chemical treatments by using a 6 M HCl acid for additional fat extraction. Finally, this approach allowed to significantly reduce the environmental impact of solid waste, decreasing also the costs associated with disposal, while contributing to the circular economy of the tanning sector. (C) 2020 TheAuthor(s). Published by Elsevier Ltd.
引用
收藏
页码:381 / 390
页数:10
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