Microstructural characterization of Y2O3 ODS-Fe-Cr model alloys

被引:43
作者
de Castro, V. [1 ]
Leguey, T. [2 ]
Munoz, A. [2 ]
Monge, M. A. [2 ]
Pareja, R. [2 ]
Marquis, E. A. [1 ]
Lozano-Perez, S. [1 ]
Jenkins, M. L. [1 ]
机构
[1] Univ Oxford, Dept Mat, Oxford OX1 3PH, England
[2] Univ Carlos III Madrid, Dept Fis, Leganes 28911, Spain
基金
英国工程与自然科学研究理事会;
关键词
STEEL; EUROFER-97; DISPERSION;
D O I
10.1016/j.jnucmat.2008.12.136
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Two Fe-12 wt% Cr alloys, one containing 0.4 wt% Y2O3 and the other Y2O3-free, have been produced by mechanical alloying followed by hot isostatic pressing. These oxide dispersion strengthened and reference alloys were characterized both in the as-HIPed state and after tempering by transmission electron microscopy and atom-probe tomography. The as-HIPed alloys exhibited the characteristic microstructure of lath martensite and contained a high density of dislocations. Small voids with sizes <10 nm were also observed. Both alloys also contained M3C and M23C6 carbides (M = Cr, Fe) probably as a result of C ingress during milling. After tempering at 1023 K for 4 h the microstructures had partially recovered. In the recovered regions, martensite laths were replaced by equiaxed grains in which M23C6 carbides decorated the grain boundaries. In the ODS alloy nanoparticles containing Y were commonly observed within grains, although they were also present at grain boundaries and adjacent to large carbides. (C) 2009 Elsevier B.V. All rights reserved.
引用
收藏
页码:449 / 452
页数:4
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