Development of Al2O3-TiO2 composite ceramics for high-power millimeter-wave applications

被引:23
作者
Kolodiazhnyi, T. [1 ]
Annino, G. [2 ]
Spreitzer, M. [3 ]
Taniguchi, T. [1 ]
Freer, R. [4 ]
Azough, F. [4 ]
Panariello, A. [5 ]
Fitzpatrick, W. [5 ]
机构
[1] Natl Inst Mat Sci, Tsukuba, Ibaraki 3050044, Japan
[2] CNR, Ist Proc Chim Fis, I-56124 Pisa, Italy
[3] Jozef Stefan Inst, Ljubljana 1000, Slovenia
[4] Univ Manchester, Sch Mat, Ctr Mat Sci, Manchester M1 7HS, Lancs, England
[5] COMDEV Int, Corp R&D Ctr, Cambridge, ON N1R 7H6, Canada
基金
英国工程与自然科学研究理事会;
关键词
Dielectric resonator; Dielectric loss; Composite ceramics; Microwaves; DIELECTRIC LOSS; TEMPERATURE-COEFFICIENT; DEFECT STRUCTURE; RESONATORS;
D O I
10.1016/j.actamat.2009.03.050
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Al2O3-TiO2 composite dielectric ceramics have been prepared by different sintering techniques including high-temperature, high-pressure sintering (2.5 GPa, T = 1000 degrees C) and conventional pressureless sintering (T = 1350 degrees C). Formation of the Al2TiO5 secondary phase has been completely suppressed by optimization of the sintering and annealing temperatures. Dielectric properties were measured in the 10-11 GHz range using the cylindrical resonant cavity technique and in the 40-92 GHz range using the open resonator whispering gallery mode technique. At 10 GHz, the optimized composite material (0.895 Al2O3-0.105 TiO2) exhibited Q x f = 210 THz, epsilon' = 12.5 and tau(f) = +2.0 ppm K-1 at room temperature. As an evidence of an additional, low-frequency (possibly Debye-type), extrinsic contribution to the dielectric loss, the Q x f value gradually increased with frequency and reached a plateau of Q x f approximate to 340 THz at approximately 80 GHz. It is demonstrated that Al2O3-TiO2 composites have considerable potential as dielectric resonators in the output multiplexers of communication satellites. (C) 2009 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
引用
收藏
页码:3402 / 3409
页数:8
相关论文
共 18 条
[1]   Sintered alumina with low dielectric loss [J].
Alford, NM ;
Penn, SJ .
JOURNAL OF APPLIED PHYSICS, 1996, 80 (10) :5895-5898
[2]   Layered Al2O3-TiO2 composite dielectric resonators with tuneable temperature coefficient for microwave applications [J].
Alford, NMN ;
Breeze, J ;
Penn, SJ ;
Poole, M .
IEE PROCEEDINGS-SCIENCE MEASUREMENT AND TECHNOLOGY, 2000, 147 (06) :269-273
[3]   Open resonators for millimeter wave spectroscopy [J].
Annino, G. ;
Kolodiazhnyi, T. ;
Martinelli, M. .
SIXTH INT KHARKOV SYMPOSIUM ON PHYSICS AND ENGINEERING OF MICROWAVES, MILLIMETER AND SUBMILLIMETER WAVES/WORKSHOP ON TERAHERTZ TECHNOLOGIES, VOLS 1 AND 2, 2007, :109-+
[4]   Dielectric properties of materials using whispering gallery dielectric resonators: Experiments and perspectives of ultra-wideband characterization [J].
Annino, G ;
Bertolini, D ;
Cassettari, M ;
Fittipaldi, M ;
Longo, I ;
Martinelli, M .
JOURNAL OF CHEMICAL PHYSICS, 2000, 112 (05) :2308-2314
[5]   Microwave dielectric loss in oxides: Theory and experiment [J].
Aupi, X ;
Breeze, J ;
Ljepojevic, N ;
Dunne, LJ ;
Malde, N ;
Axelsson, AK ;
Alford, NM .
JOURNAL OF APPLIED PHYSICS, 2004, 95 (05) :2639-2645
[6]   Ultralow loss polycrystalline alumina [J].
Breeze, JD ;
Aupi, X ;
Alford, NM .
APPLIED PHYSICS LETTERS, 2002, 81 (26) :5021-5023
[7]   Crystal growth and defect structure of Al3+-doped rutile [J].
Gesenhues, U ;
Rentschler, T .
JOURNAL OF SOLID STATE CHEMISTRY, 1999, 143 (02) :210-218
[8]   INTRINSIC DIELECTRIC LOSS IN CRYSTALS [J].
GUREVICH, VL ;
TAGANTSEV, AK .
ADVANCES IN PHYSICS, 1991, 40 (06) :719-767
[9]  
JACKSON JD, 1998, CLASSICAL ELECTRODYN, P158
[10]   Equation for the effective permittivity of particle-filled composites for material design applications [J].
Jylha, Liisi ;
Sihvola, Ari .
JOURNAL OF PHYSICS D-APPLIED PHYSICS, 2007, 40 (16) :4966-4973