Crystal structure of bis(acetonitrile)bis[μ-(benzylthiolato)]hexacarbonyl-di(molybdenum), [Mo(CO)3(SCH2C6H5)(CH3CN)]2

被引：0

作者：

Walters, MA

Sireci, A

Incarvito, CD

Rheingold, AL

机构：

[1] NYU, Dept Chem, New York, NY 10003 USA

[2] Univ Delaware, Dept Chem, Newark, DE 19716 USA

来源：

ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2002年 / 217卷 / 02期

关键词：

D O I：

暂无

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

C24H20Mo2N2O6S2, orthorhombic, Pbca (No. 61), a = 11.104(2) Angstrom, b = 12.424(2) Angstrom, c = 19.332(3) Angstrom, V = 2666.9 Angstrom(3), Z = 4, R-gt(F) = 0.057, wR(ref)(F-2) = 0.158, T = 173 K.

引用

页码：271 / 272

页数：2

共 9 条

[1] Synthesis and characterization of [Mo(μ-EPh)(CO)3(CH3CN)]2 (E = Se, Te), including the X-ray structure of the tellurium derivative [J].

Carey, J ;

Fettinger, JC ;

Poli, R ;

Smith, KM .

INORGANICA CHIMICA ACTA, 2000, 299 (01) :118-122

[2] FORMATION OF CLUSTERS BY OXIDATIVE ADDITION OF ORGANIC AND INORGANIC DISULFIDES - MOLECULAR-STRUCTURES OF (MECN)2(CO)6MO2(MU-SPH)2 AND MO2FE7S8(CO)22 [J].

EREMENKO, IL ;

PASYNSKII, AA ;

ABDULAEV, AS ;

ALIEV, AS ;

ORAZSAKHATOV, B ;

SLEPTSOVA, SA ;

NEKHAEV, AI ;

SHKLOVER, VE ;

STRUCHKOV, YT .

JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1989, 365 (03) :297-307

[3]

JOWITT RN, 1968, INORG NUCL CHEM LETT, V4, P39

[4] VERSATILITY OF MO(TERT-BUS)4 - SELECTIVE FORMATION OF A SERIES OF THIOLATOMOLYBDENUM(I), THIOLATOMOLYBDENUM(II), AND THIOLATOMOLYBDENUM(IV) COMPOUNDS [J].

KAMATA, M ;

YOSHIDA, T ;

OTSUKA, S ;

HIROTSU, K ;

HIGUCHI, T .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1981, 103 (12) :3572-3574

[5]

NEFEDOV SE, 1992, ZH NEORG KHIM+, V37, P335

[6]

Sheldrick G.M., 1990, SHELXS 97 PROGRAM SO

[7]

Sheldrick G.M., 1993, PROGRAM CRYSTAL STRU

[8] 2-ELECTRON TRANSFER ACCOMPANIED BY METAL METAL BOND FORMATION - SYNTHESIS AND ELECTROCHEMISTRY OF DINUCLEAR MOLYBDENUM AND TUNGSTEN CARBONYL THIOLATES [J].

SMITH, DA ;

ZHUANG, B ;

NEWTON, WE ;

MCDONALD, JW ;

SCHULTZ, FA .

INORGANIC CHEMISTRY, 1987, 26 (15) :2524-2531

[9]

ZHUANG B, 1986, INORG CHIM ACTA, V116, pL41

← 1 →