X-ray diffraction analysis of (Ph2PO)2

被引：0
作者：
Gao, Wei [1 ]
Sun, De-Mei [1 ]
Sun, Yan-Jun [1 ]
机构：
[1] Henan Univ Tradit Chinese Med, Sch Pharm, Zhengzhou 450046, Peoples R China
来源：
MOLECULAR CRYSTALS AND LIQUID CRYSTALS | 2016年 / 624卷 / 01期
基金：
中国国家自然科学基金;
关键词：
phosphine; diphenyl; Crystal structure; DIIRON DITHIOLATE COMPLEX; CRYSTAL-STRUCTURE; STRUCTURAL-CHARACTERIZATION; BIOLOGICAL-ACTIVITY; DIPHOSPHINE LIGAND; TRIPHENYLPHOSPHINE;
D O I：
10.1080/15421406.2015.1044716
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The title compound (Ph2PO)2 is analyzed by single crystal X-ray diffraction analysis. The crystals are monoclinic, space group P2(1)/n with a = 9.5112(19) angstrom, b = 11.161(2) angstrom, c = 9.5487(19) angstrom, alpha = 90 degrees, beta = 91.65(3)degrees, gamma = 90 degrees, V = 1013.2(3) angstrom(3), Z = 2, F((000))=420, Dc = 1.319g cm(-3), mu = 0.232mm(-1), the final R = 0.0818, and wR=0.2259. A total of 7954 reflections were collected, of which 1758 were independent (R-int=0.0542). In the crystal packing diagram, intermolecular C-H center dot center dot center dot O hydrogen bonds stabilize the solid state of the title compound.
引用
收藏
页码：271 / 274
页数：4
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