The synthesis of the first acetylenic silyl derivatives of 2-methylimidazole and benzimidazole

被引：5

作者：

Yarosh, N. O. ^{[1
]}

Zhilitskaya, L. V. ^{[1
]}

Shagun, L. G. ^{[1
]}

Larina, L. I. ^{[1
]}

Dorofeev, I. D. ^{[1
]}

机构：

[1] Russian Acad Sci, Favorskii Irkutsk Inst Chem, Siberian Branch, Irkutsk 664033, Russia

来源：

RUSSIAN JOURNAL OF GENERAL CHEMISTRY | 2015年 / 85卷 / 10期

关键词：

1,3-bis(iodomethyl)tetramethyldisilylethyne; 2-methylimidazole; benzimidazole; alkylation; iodides; ONE-POT SYNTHESIS; IONIC LIQUID; IMIDAZOLE; ALKYLATION; SOLVENT; AGENTS;

D O I：

10.1134/S1070363215100151

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The earlier unknown acetylenic silyl iodides of linear and cyclic structure form in the reaction of 2-methylimidazole and benzimidazole with bis[dimethyl(iodomethyl)silyl]ethyne. The synthesized compounds are characterized by the data of elemental analysis, (1)De, D-13, N-15, Si-29 NMR, IR, Raman and UV spectroscopy.

引用

页码：2304 / 2308

页数：5

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