Influence of Sample Pretreatment on the Analysis of High Contents of Rare-Earth and High Field Strength Elements in Geological Samples by ICP-AES and ICP-MS (Case Study of the Tomtor Deposit)

被引：2

作者：

Saryg-ool, Bagai-ool Yu ^{[1
]}

Bukreeva, Lidiya N. ^{[1
]}

Myagkaya, Irina N. ^{[1
]}

Tolstov, Aleksandr, V ^{[2
]}

Lazareva, Elena, V ^{[1
]}

Zhmodik, Sergey M. ^{[1
]}

机构：

[1] Sobolev Inst Geol & Mineral SB RAS, Novosibirsk, Russia

[2] PJSC ALROSA, Mirny, Republic Of Sak, Russia

来源：

JOURNAL OF SIBERIAN FEDERAL UNIVERSITY-CHEMISTRY | 2020年 / 13卷 / 04期

基金：

俄罗斯科学基金会;

关键词：

Tomtor; rare earth elements; high field strength elements; sample preparation; fusion; acid; digestion; INDUCTIVELY-COUPLED PLASMA; ATOMIC-EMISSION-SPECTROMETRY; ORES; REE; SEDIMENTS; HEALTH; VEPP-3; NB;

D O I：

10.17516/1998-2836-0208

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Influence of sample pretreatment on the analysis of the high contents of rare earth (REE) and high field strength (HFSE) elements in geological samples by inductively coupled plasma atomic emission spectrometry (ICP-AES) and inductively coupled plasma mass spectrometry (ICP-MS) was studied. The rocks and rich ores of the Tomtor Nb-REE deposit were explored. Complete dissolution of the geological samples with a high content of "refractory" minerals has been achieved using fusion with a sodium peroxide. The results obtained by ICP-AES and ICP-MS after chemical dissolution are comparable with the results obtained by the XRF-SR without chemical pretreatment.

引用

页码：593 / 605

页数：13

共 5 条

[1] SAMPLE PREPARATION FOR DETERMINATION OF RARE EARTH ELEMENTS IN GEOLOGICAL SAMPLES BY ICP-MS: A CRITICAL REVIEW
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[2] Determination of rare earth elements in Indian coastal monazite by ICP-AES and ICP-MS analysis and their geochemical significance
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[5] Determination of Rare Earth Elements in Natural Water Samples by Rapid Sequential High-Resolution Continuum Source Flame Atomic Absorption Spectrometry (HR CS FAAS) and inductively Coupled Plasma-Mass Spectrometry (ICP-MS)
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ANALYTICAL LETTERS, 2019, 52 (13) : 2057 - 2068

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