Determining hydrogen-bond strengths in the solid state by NMR:: the quantitative measurement of homonuclear J couplings

被引:107
作者
Brown, SP
Pérez-Torralba, M
Sanz, D
Claramunt, RM
Emsley, L [1 ]
机构
[1] Ecole Normale Super Lyon, CNRS, ENS, UMR 5532,Lab Stereochim & Interact Mol, F-69364 Lyon, France
[2] Univ Nacl Educ Distancia, Fac Ciencias, Dept Quim Organ & Biol, Madrid 28040, Spain
关键词
D O I
10.1039/b205324a
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Hydrogen-bonding strengths in the solid state are quantitatively determined by the accurate measurement of (15)N-(15)N J couplings using a straightforward 2D MAS NMR spin-echo approach.
引用
收藏
页码:1852 / 1853
页数:2
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