Bio-inspired green synthesis of Fe3O4 spherical magnetic nanoparticles using Syzygium cumini seed extract

被引:114
|
作者
Venkateswarlu, Sada [1 ]
Kumar, B. Natesh [1 ]
Prasad, C. H. [1 ]
Venkateswarlu, P. [1 ]
Jyothi, N. V. V. [1 ]
机构
[1] Sri Venkateswara Univ, Dept Chem, Analyt & Inorgan Div, Tirupati 517502, Andhra Pradesh, India
关键词
S. cumini seed extract; Spherical magnetic nanoparticles; XRD; TEM; FTIR; VSM; SOLID-PHASE EXTRACTION; L; SKEELS; DRUG; NANOWIRES; OXIDE; RELEASE;
D O I
10.1016/j.physb.2014.04.031
中图分类号
O469 [凝聚态物理学];
学科分类号
070205 ;
摘要
A novel and bio-inspired Fe3O4 spherical magnetic nanoparticles (SMNPs) were synthesized using Syzygium cumini (S. cumini) seed extract, which is a non-toxic ecofriendly fruit waste material. S. cumini seed extract acts as a green solvent, reducing and capping agent in which sodium acetate acts as electrostatic stabilizing agent. The green synthesized nanoparticles were characterized with the help of various techniques such as X-ray diffraction (XRD), Raman spectroscopy, transmission electron microscopy (TEM), Energy-dispersive spectroscopy (EDS), Vibrating sample magnetometer (VS M), FTIR spectroscopy and nitrogen adsorption and desorption analysis techniques. The XRD study divulged that the synthesized SMNPs have inverse spinel cubic structure. The hysteresis loop of Fe3O4 nanoparticles shows an excellent ferromagnetic behavior with saturation magnetization value of 13.6 emu/g. (C) 2014 Elsevier B.V. All rights reserved.
引用
收藏
页码:67 / 71
页数:5
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