Synthesis and Crystal Growth of Tetragonal β-Fe1.00Se

被引:40
作者
Koz, Cevriye [1 ]
Schmidt, Marcus [1 ]
Borrmann, Horst [1 ]
Burkhardt, Ulrich [1 ]
Roessler, Sahana [1 ]
Carrillo-Cabrera, Wilder [1 ]
Schnelle, Walter [1 ]
Schwarz, Ulrich [1 ]
Grin, Yuri [1 ]
机构
[1] Max Planck Inst Chem Phys Fester Stoffe, D-01187 Dresden, Germany
来源
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE | 2014年 / 640卷 / 8-9期
关键词
Chemical vapor transport; Superconductivity; Selenium; Iron; IRON; SUPERCONDUCTIVITY; FE3SE4; FESE; SE;
D O I
10.1002/zaac.201300670
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
Single crystals of tetragonal beta-Fe1.00Se were grown from polycrystalline material by chemical vapor transport reaction at temperatures below 723 K using AlCl3 as transport additive. The plate-shaped single crystals have edge lengths up to 4 mm. The single crystals display complete diamagnetic shielding 4 pi chi approximate to -1 below the super-conducting transition.
引用
收藏
页码:1600 / 1606
页数:7
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