Evolution of Helium Bubbles and Discs in Irradiated 6H-SiC during Post-Implantation Annealing

被引:21
作者
Shen, Qiang [1 ]
Zhou, Wei [2 ]
Ran, Guang [1 ]
Li, Ruixiang [1 ]
Feng, Qijie [2 ]
Li, Ning [1 ]
机构
[1] Xiamen Univ, Coll Energy, Xiamen 361102, Fujian, Peoples R China
[2] China Acad Engn Phys, Mianyang 621900, Sichuan, Peoples R China
来源
MATERIALS | 2017年 / 10卷 / 02期
关键词
SiC; irradiation; annealing; bubble growth; microstructure; ELECTRON-MICROSCOPY; SILICON-CARBIDE; METALS; IMPLANTATION; DIFFUSION; CAVITIES; REACTORS; STRAIN; DAMAGE; WATER;
D O I
10.3390/ma10020101
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
The single crystal 6H-SiC with [0001] crystal direction irradiated by 400 keV He+ ions with 1 x 10(17) ions/cm(2) fluence at 400 degrees C were annealed at 600, 900, 1200 and 1400 degrees C for different durations. The evolution of helium bubbles and discs was investigated by transmission electron microscopy. An irradiated layer distributed with fine helium bubbles was formed with a width of similar to 170 nm after helium ion irradiation. The size of gas bubbles increased with increasing annealing time and temperature and finally reached stable values at a given annealing temperature. According to the relationship between the bubble radii and annealing time, an empirical formula for calculating the bubble radii at the annealing temperature ranged from 600 to 1400 degrees C was given by fitting the experiment data. Planar bubble clusters (discs) were found to form on (0001) crystal plane at both sides of the bubble layer when the annealing temperature was at the range of 800-1200 degrees C. The mechanism of bubble growth during post-implantation annealing and the formation of bubble discs were also analyzed and discussed.
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页数:8
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