Determination of polyaromatic hydrocarbons in coal tar pitch

被引:15
作者
Afanasov, I. M. [1 ]
Kepman, A. V. [1 ]
Morozov, V. A. [1 ]
Seleznev, A. N. [1 ]
Avdeev, V. V. [1 ]
机构
[1] Moscow MV Lomonosov State Univ, Dept Chem, Moscow 119992, Russia
关键词
POLYCYCLIC AROMATIC-HYDROCARBONS; POLYCHLORINATED-BIPHENYLS; EXTRACTION PROCEDURE; MASS-SPECTROMETRY; DEGRADATION; AIR; SEDIMENTS; WATERS; GC/MS; MODEL;
D O I
10.1134/S1061934809040078
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Different techniques for extracting polyaromatic hydrocarbons (PAHs) from coal tar pitch for their quantitative determination by gas chromatography-mass spectrometry are compared. It has been found that the ultrasonic treatment of a sample allowed the quantitative extraction of PAHs from coal tar pitch. The results of the quantitative determination of PAHs in samples of coal tar pitch obtained by Soxhlet extraction and liquid-liquid extraction with ultrasonic treatment agree within the experimental error range.
引用
收藏
页码:361 / 365
页数:5
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