Synthesis and Structural Characterizations of meso-Tetraphenyl Porphyrin

被引：1
|
作者：
Zhao, Tianxiang [1 ]
Zhang, Jianbin [1 ,2 ]
Yang, Xiaoxia [1 ]
Xu, Qiuxia [1 ]
Lan, Gongjia [1 ]
机构：
[1] Inner Mongolia Univ Technol, Coll Chem Engn, Hohhot 010051, Peoples R China
[2] Peking Univ, Dept Appl Chem, Coll Chem & Mol Engn, Beijing 100871, Peoples R China
来源：
ASIAN JOURNAL OF CHEMISTRY | 2014年 / 26卷 / 10期
关键词：
Tetraphenylporphyrin; Recrystallization; Structural characterization;
D O I：
10.14233/ajchem.2014.16659
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
In this paper tetraphenyl porphyrin (H2TPP) was synthesized by using pyrrole and benzaldehyde as raw materials under the catalysis of I p-nitrobenzoic acid the prepared tetraphenyl porphyrin Was re crystallized in a mixed system of methanol and methylene, chloride (CH2Cl2) and the yield of tetraphenyl porphyrin is 34.2 %. Tetraphenyl porphyrin was characterized by using FTIR, UV-visible, H-1 NMR and fluorescence spectrophotometer. The effects on the yield of tetraphenyl porphyrin at different volumes of dimethylbenzene as solvent were explored.
引用
收藏
页码：3050 / 3052
页数：3
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