Determination of elements in Euonymus alatus by microwave digestion-ICP-AES

被引:0
作者
Tang Rui [1 ]
Hou Xiang-Yan [1 ]
Sun Chen [1 ]
Yang Yi [1 ]
机构
[1] Beijing Univ Chem Technol, Beijing 100029, Peoples R China
关键词
microwave digestion; AAS; ICP-AES; Euonymus alatus; trace elements;
D O I
暂无
中图分类号
O433 [光谱学];
学科分类号
0703 ; 070302 ;
摘要
The determination of elements in Euonymus alatus by ICP-AES was carried out in the present paper. The Euonymus alatus samples were digested by microwave digestion technique. The optimized conditions of microwave digestion procedure obtained by orthogonal array design were as follows: the volume ratio of HNO3-HCl is 2 : 1; the ratio of liquid/solid is 100 : 1; the sample particle size is 100-140 mesh. ICP-AES method was applied to the determination of ten trace elements in the sample, and was compared with AAS. The results showed that the method was rapid and simple with the relative standard deviations between 0.5%-6.2%, and the recovery between 85.5% and 105.6%.
引用
收藏
页码:1543 / 1546
页数:4
相关论文
共 10 条
[1]  
DONG LL, 2000, INFORM TRADTIONAL CH, P16
[2]  
GUO MD, 2002, PHYS TESTING CHEM B, V38, P158
[3]  
PENG XZ, 2003, HUMAN GUIDING J TRAD, V9, P54
[4]  
[王刚 Wang Gang], 2002, [药物分析杂志, Chinese Journal of Pharmaceutical Analysis], V22, P151
[5]  
Yang Y, 2004, SPECTROSC SPECT ANAL, V24, P1672
[6]  
YAO ZP, 2000, CHINESE J INFORMATIO, V7, P31
[7]  
Yi XP, 2004, SPECTROSC SPECT ANAL, V24, P890
[8]   Sub-signature operators, η-invariants and a Riemann-Roch theorem for flat vector bundles [J].
Zhang, WP .
CHINESE ANNALS OF MATHEMATICS SERIES B, 2004, 25 (01) :7-36
[9]  
Zhang Y, 2004, CHINESE J BASIC MED, V10, P67
[10]  
Zhu JY, 2003, SPECTROSC SPECT ANAL, V23, P380