Effect of Polyimide-Phosphating Double Coating and Annealing on the Magnetic Properties of Fe-Si-Cr SMCs

被引:14
作者
Long, Haiming [1 ]
Wu, Xiaojie [2 ]
Lu, Yunkun [1 ]
Zhang, Haifeng [1 ]
Hao, Junjie [1 ]
机构
[1] Univ Sci & Technol Beijing, Inst Adv Mat & Technol, Beijing 100083, Peoples R China
[2] Avic Chengdu Caic Elect Co Ltd, Chengdu 610091, Peoples R China
关键词
Fe-Si-Cr SMCs; PI; core-shell double coating; annealing; magnetic properties; ELECTROMAGNETIC PROPERTIES; ALLOY POWDERS; COMPOSITES; MICROSTRUCTURE; PARTICLES; CORES;
D O I
10.3390/ma15093350
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Fe-Si-Cr soft magnetic powder cores (SMCs), with high electrical resistivity, magnetic permeability, saturation magnetic induction, and good corrosion resistance, are widely applied to inductors, filters, choke coils, etc. However, with the development of electronic technology with high frequency and high power density, the relative decline in the magnetic properties limits the high-frequency application of SMCs. In this paper, the phosphating process and polyimide (PI) insulation coating is applied to Fe-Si-Cr SMCs to reduce the core loss, including hysteresis loss and eddy current loss. The microstructure and composition of Fe-Si-Cr powders were analyzed by SEM, XRD, and Fourier-transform infrared spectra, respectively. The structural characteristics of the Fe-Si-Cr @ phosphate layer @ PI layer core-shell double coating were studied, and the best process parameters were determined through experiments. For SMCs with 0.4 wt% content of PI, the relative permeability is greater than 68%, and the core loss is the lowest, 7086 mW/cm(3); annealed at 500 degrees C, the relative permeability is greater than 57%, and the core loss is the lowest, 6222 mW/cm(3). A 0.4 wt% content of PI, annealed at 500 degrees C, exhibits the ideal magnetic properties: mu(e) = 47 H/m, P = 6222 mW/cm(3).
引用
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页数:14
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