Ultrasound-promoted scavenging: a rapid parallel purification for solution phase combinatorial synthesis

被引:0
|
作者
Peng, YQ [1 ]
Song, GH [1 ]
Xu, XY [1 ]
机构
[1] E China Univ Sci & Technol, Inst Pesticides & Pharmaceut, Shanghai Key Lab Chem Biol, Shanghai 200237, Peoples R China
关键词
combinatorial chemistry; purification; scavenger; sonication; isothiocyanates;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Ultrasound irradiation enhances the mass transfer and reaction rate in scavenging, avoiding the trouble of time-consuming purification procedure in solution-phase parallel synthesis. An application of this technique is demonstrated in the scavenging of excess isothiocyanates from reaction mixtures.
引用
收藏
页码:261 / 263
页数:3
相关论文
共 29 条
  • [1] Ultrasound-promoted synthesis of novel 2-chloroquinolin-4-pyrimidine carboxylate derivatives as potential antibacterial agents
    Balaji, G. L.
    Rajesh, K.
    Ali, Shabana Kouser
    Vijayakumar, V.
    RESEARCH ON CHEMICAL INTERMEDIATES, 2013, 39 (04) : 1807 - 1815
  • [2] Ultrasound-promoted synthesis of novel 2-chloroquinolin-4-pyrimidine carboxylate derivatives as potential antibacterial agents
    G. L. Balaji
    K. Rajesh
    Shabana Kouser Ali
    V. Vijayakumar
    Research on Chemical Intermediates, 2013, 39 : 1807 - 1815
  • [3] Low-temperature ultrasound-promoted synthesis of Cr-TiO2-supported photocatalysts for valorization of glucose and phenol degradation from liquid phase
    Colmenares, Juan C.
    Magdziarz, Agnieszka
    Kurzydlowski, Krzysztof
    Grzonka, Justyna
    Chernyayeva, Olga
    Lisovytskiy, Dmytro
    APPLIED CATALYSIS B-ENVIRONMENTAL, 2013, 134 : 136 - 144
  • [4] Solution-phase parallel oxazole synthesis with TosMIC
    Kulkarni, BA
    Ganesan, A
    TETRAHEDRON LETTERS, 1999, 40 (30) : 5637 - 5638
  • [5] Monitoring solution-phase combinatorial library synthesis by capillary electrophoresis
    Gaus, HJ
    Kung, PP
    Brooks, D
    Cook, PD
    Cummins, LL
    BIOTECHNOLOGY AND BIOENGINEERING, 1998, 61 (03) : 169 - 177
  • [6] Microwave-Assisted Solid-phase Synthesis (MASS): Parallel and Combinatorial Chemical Library Synthesis
    Al-Obeidi, Fahad
    Austin, Richard E.
    Okonya, John F.
    Bond, Daniel R. S.
    MINI-REVIEWS IN MEDICINAL CHEMISTRY, 2003, 3 (05) : 449 - 460
  • [7] A general Staudinger protocol for solution-phase parallel synthesis
    Lindsley, CW
    Zhao, Z
    Newton, RC
    Leister, WH
    Strauss, KA
    TETRAHEDRON LETTERS, 2002, 43 (25) : 4467 - 4470
  • [8] Fluorous-tethered quenching reagents for solution phase parallel synthesis
    Lindsley, CW
    Zhao, Z
    Leister, WH
    TETRAHEDRON LETTERS, 2002, 43 (23) : 4225 - 4228
  • [9] A straightforward protocol for the solution-phase parallel synthesis of ceramide analogues
    Grijalvo, Santiago
    Matabosch, Xavier
    Llebaria, Amadeu
    Delgado, Antonio
    EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2008, 2008 (01) : 150 - 155
  • [10] Amino-functionalized carbon nanotubes as nucleophilic scavengers in solution phase combinatorial synthesis
    Li, Yongsheng
    Zhao, Yuzeng
    Zhang, Zhuo
    Xu, Yaomin
    TETRAHEDRON LETTERS, 2010, 51 (10) : 1434 - 1436