Additive manufactured porous titanium structures: Through-process quantification of pore and strut networks

被引:97
作者
Kim, Taek Bo [1 ]
Yue, Sheng [2 ]
Zhang, Ziyu [1 ]
Jones, Eric [3 ]
Jones, Julian R. [1 ]
Lee, Peter D. [2 ]
机构
[1] Univ London Imperial Coll Sci Technol & Med, Dept Mat, London SW7 2AZ, England
[2] Univ Manchester, Sch Mat, Manchester M13 9PL, Lancs, England
[3] Univ Liverpool, Ctr Mat & Struct, Liverpool L69 3GH, Merseyside, England
基金
英国工程与自然科学研究理事会;
关键词
Additive manufacturing; Selective laser melting; X-ray microtomography; Porous titanium; Quantification methods; TISSUE SCAFFOLDS; FOAMS; MICROTOMOGRAPHY; IMAGES; IMPACT; SPACE; JET;
D O I
10.1016/j.jmatprotec.2014.05.006
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Titanium and its alloys are successfully used in aerospace through to marine applications. Selective laser melting (SLM) is an additive manufacturing technique, which promises to allow production of novel Ti structures. However, there is still a paucity of accepted methods for quantifying build quality. The viability of using X-ray microtomography (mu CT) to quantify and track changes in morphology of SLM Ti porous structures at each stage of the post-laser melting production was tested, quantifying its quality through process. Quantification was achieved using an accessible volume tool to determine pore and strut sizes. Removal of partially sintered struts by cleaning was visualised and quantified. Eighty-eight percent of the struts broken by the cleaning process were found to have connecting neck diameters of less than 180 mu m with a mean of 109 mu m allowing build criteria to be set. Tracking particles removed during cleaning revealed other methods to improve build design, e.g. avoiding low angle struts that did not sinter well. Partially melted powder particles from strut surfaces were quantified by comparing surface roughness values at each cleaning step. The study demonstrates that mu CT provides not only 3D quantification of structure quality, but also a feedback mechanism, such that improvements to the initial design can be made to create more stable and reliable titanium structures for a wide variety of applications. (C) 2014 The Authors. Published by Elsevier B.V. This is an open access article under the CC BY license (http://creativecommons.org/licenses/by/3.0/).
引用
收藏
页码:2706 / 2715
页数:10
相关论文
共 28 条
[1]  
[Anonymous], J SOLID MECH MAT ENG
[2]  
[Anonymous], 2000, MEDICAL IMAGE COMPUT
[3]   Analysis of pore interconnectivity in bioactive glass foams using X-ray microtomography [J].
Atwood, RC ;
Jones, JR ;
Lee, PD ;
Hench, LL .
SCRIPTA MATERIALIA, 2004, 51 (11) :1029-1033
[4]   Additively manufactured cellular structures: Impact of microstructure and local strains on the monotonic and cyclic behavior under uniaxial and bending load [J].
Brenne, F. ;
Niendorf, T. ;
Maier, H. J. .
JOURNAL OF MATERIALS PROCESSING TECHNOLOGY, 2013, 213 (09) :1558-1564
[5]   METALLIC FOAMS - THEIR PRODUCTION, PROPERTIES AND APPLICATIONS [J].
DAVIES, GJ ;
ZHEN, S .
JOURNAL OF MATERIALS SCIENCE, 1983, 18 (07) :1899-1911
[6]   Processing of titanium foams [J].
Dunand, DC .
ADVANCED ENGINEERING MATERIALS, 2004, 6 (06) :369-376
[7]   Selective Electron Beam Melting of Cellular Titanium: Mechanical Properties [J].
Heinl, Peter ;
Koerner, Carolin ;
Singer, Robert F. .
ADVANCED ENGINEERING MATERIALS, 2008, 10 (09) :882-888
[8]   Non-destructive quantitative 3D analysis for the optimisation of tissue scaffolds [J].
Jones, Julian R. ;
Poologasundarampillai, Gowsihan ;
Atwood, Robert C. ;
Bernard, Dominique ;
Lee, Peter D. .
BIOMATERIALS, 2007, 28 (07) :1404-1413
[9]   Quantifying the 3D macrostructure of tissue scaffolds [J].
Jones, Julian R. ;
Atwood, Robert C. ;
Poologasundarampillai, Gowsihan ;
Yue, Sheng ;
Lee, Peter D. .
JOURNAL OF MATERIALS SCIENCE-MATERIALS IN MEDICINE, 2009, 20 (02) :463-471
[10]   Validation of x-ray microfocus computed tomography as an imaging tool for porous structures [J].
Kerckhofs, G. ;
Schrooten, J. ;
Van Cleynenbreugel, T. ;
Lomov, S. V. ;
Wevers, M. .
REVIEW OF SCIENTIFIC INSTRUMENTS, 2008, 79 (01)