3-Methyl-3a,4-Dihydro-3H-Thiochromeno[4,3-c]isoxazol

被引：0

作者：

Bennani, Brahim ^{[2
]}

Kerbal, Abdelali ^{[2
]}

El-Bali, Brahim ^{[3
]}

Bolte, Michael ^{[1
]}

机构：

[1] Univ Frankfurt, Inst Anorgan Chem, D-60438 Frankfurt, Germany

[2] Univ Sidi Mohammed Ben Abdelah, Chim Organ Lab, Fac Sci, Atlas 1796, Fes, Morocco

[3] Univ Mohamed I, Lab Mineral Solid & Analyt Chem, Dept Chem, Fac Sci, Oujda 60000, Morocco

来源：

JOURNAL OF CHEMICAL CRYSTALLOGRAPHY | 2009年 / 39卷 / 06期

关键词：

Cycloaddition reaction; Single crystal structure; Weak hydrogen bond; pi-Stacking interaction;

D O I：

10.1007/s10870-009-9552-x

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The crystal structure of the title compound, C11H11NOS, was determined by an X-ray diffraction analysis. The compound crystallizes in the monoclinic space group P2(1)/c with cell parameters a = 10.533(2) angstrom, b = 12.7826(19) angstrom, c = 7.6491(17) angstrom, beta = 107.997(17)degrees, V = 979.5(3) angstrom(3) and Z = 4. The S containing heterocycle adopts a sofa conformation, whereas the 5-membered ring adopts an envelope conformation. The crystal packing is characterized by weak C-H center dot center dot center dot N contacts and pi-stacking interactions.

引用

页码：466 / 468

页数：3

共 15 条

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