(Z)-2-(1-(5-Methyl-1-(4-nitrophenyl)-1H-1,2,3-triazol-4-yl)ethylidene)-N-phenylhydrazine-1-carbothioamide

被引：2
|
作者：
Kariuki, Benson M. [1 ]
Abdel-Wahab, Bakr F. [2 ]
Bekheit, Mohamed S. [3 ]
El-Hiti, Gamal A. [4 ]
机构：
[1] Cardiff Univ, Sch Chem, Main Bldg,Pk Pl, Cardiff CF10 3AT, Wales
[2] Natl Res Ctr, Chem Ind Res Inst, Appl Organ Chem Dept, Dokki 12622, Giza, Egypt
[3] Natl Res Ctr, Dept Pesticide Chem, Dokki 12622, Giza, Egypt
[4] King Saud Univ, Coll Appl Med Sci, Cornea Res Chair, Dept Optometry, Riyadh 11433, Saudi Arabia
来源：
MOLBANK | 2022年 / 2022卷 / 04期
关键词：
synthesis; 1; 2; 3-triazole; N-phenylhydrazinecarbothioamide; X-ray diffraction; heterocycles; hydrazones; CRYSTAL-STRUCTURE; THIOSEMICARBAZONES; COMPLEXES; 1,2,3-TRIAZOLE; CU(II);
D O I：
10.3390/M1462
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Reaction of equimolar equivalents of 1-(5-methyl-1-(4-nitrophenyl)-1H-1,2,3-triazol-4-yl)ethan-1-one (1) and N-phenylhydrazinecarbothioamide (2) in boiling ethanol containing a catalytic amount of concentrated hydrochloric acid for 4 h gave (Z)-2-(1-(5-methyl-1-(4-nitrophenyl)-1H-1,2,3-triazol-4-yl)ethylidene)-N-phenylhydrazine-1-carbothioamide (3) with 88% yield. The structure of 3 was established using single-crystal X-ray diffraction and magnetic resonance spectroscopy.
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页数：7
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