Sequential determination of 210Po and uranium radioisotopes in drinking water by alpha-particle spectrometry

被引:42
作者
Benedik, L. [1 ]
Vasile, M. [1 ]
Spasova, Y. [1 ]
Waetjen, U. [1 ]
机构
[1] Commiss European Communities, Joint Res Ctr, Inst Reference Mat & Measurements, B-2440 Geel, Belgium
关键词
Polonium; Uranium; Alpha-particle spectrometry; Radiochemistry; Drinking water;
D O I
10.1016/j.apradiso.2009.01.033
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
Procedures for the sequential determination of low level Po-210 and uranium radioisotopes in drinking water by alpha-particle spectrometry are presented. After addition of Po-208 and U-232 tracers, the radionuclides were preconcentrated from water samples by co-precipitation on Fe(OH)(3) or MnO2 at pH 9 using ammonia solution. The Po-210 source was prepared by spontaneous deposition onto a copper disc either before or after uranium separation. The uranium source for alpha-particle counting was prepared by micro co-precipitation with CeF3. The procedures were tested on mineral water and the results obtained are compared. (c) 2009 Elsevier Ltd. All rights reserved.
引用
收藏
页码:770 / 775
页数:6
相关论文
共 8 条
[1]  
[Anonymous], 1993, GUID DRINK WAT QUAL
[2]  
Benedik L, 2001, ACTA CHIM SLOV, V48, P199
[3]  
Benedik L., 2008, P 7 INT C NUCL RAD N
[5]   SEPARATION AND PRECONCENTRATION OF ACTINIDES FROM ACIDIC MEDIA BY EXTRACTION CHROMATOGRAPHY [J].
HORWITZ, EP ;
CHIARIZIA, R ;
DIETZ, ML ;
DIAMOND, H .
ANALYTICA CHIMICA ACTA, 1993, 281 (02) :361-372
[6]   Standardisation of low-activity actinide solutions by alpha-particle counting at a defined solid angle [J].
Sibbens, G ;
Pommé, S ;
Altzitzoglou, T .
APPLIED RADIATION AND ISOTOPES, 2004, 61 (2-3) :405-408
[7]  
SILL CW, 1981, ANAL CHEM, V53, P421
[8]  
World Health Organisation (WHO), 2006, Guidelines for Drinking-Water Quality, V1