The microstructure of mechanically alloyed Al-Mg determined by X-ray diffraction peak profile analysis

被引:68
作者
Gubicza, J
Kassem, M
Ribárik, G
Ungár, T
机构
[1] Eotvos Lorand Univ, Dept Gen Phys, H-1518 Budapest, Hungary
[2] Eotvos Lorand Univ, Dept Solid State Phys, H-1518 Budapest, Hungary
[3] Suez Canal Univ, Fac Petr & Min, Dept Mat Sci & Engn, Suez, Egypt
来源
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING | 2004年 / 372卷 / 1-2期
基金
匈牙利科学研究基金会;
关键词
Al-Mg alloys; mechanical alloying; X-ray diffraction peak profile analysis; crystallite size; dislocation structure; hardness;
D O I
10.1016/j.msea.2003.12.016
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The effect of the nominal Mg content and the milling time on the microstructure and the hardness of mechanically alloyed Al-rich Al-Mg solid solutions is studied. The crystallite size distribution and the dislocation structure are characterized by X-ray diffraction (XRD) peak profile analysis and the hardness is obtained from depth-sensing indentation tests. Magnesium gradually goes into solid solution during ball milling and after 3 h an almost complete solid solution is attained. With increasing milling time, the Mg concentration in solid solution, the dislocation density and the hardness increase, whereas the crystallite size decreases. A similar tendency of these parameters is observed at a particular duration of ball milling with increasing nominal Mg content. After 3 h milling there are no changes in both the microstructure and the hardness. (C) 2004 Elsevier B.V. All rights reserved.
引用
收藏
页码:115 / 122
页数:8
相关论文
共 50 条
[1]   Ball milling conditions for the amorphization of Zr50Cu50 [J].
Ahn, JH ;
Paek, YK .
JOURNAL OF MATERIALS SCIENCE LETTERS, 1999, 18 (01) :17-19
[2]  
BAIL AL, 1992, NIST SPEC PUBL, V846, P142
[3]   Inverse critical strains for jerky flow in Al-Mg alloys [J].
Balík, J ;
Lukác, P ;
Kubin, LP .
SCRIPTA MATERIALIA, 2000, 42 (05) :465-471
[5]   OVERVIEW NO-96 - EVOLUTION OF FCC DEFORMATION STRUCTURES IN POLYSLIP [J].
BAY, B ;
HANSEN, N ;
HUGHES, DA ;
KUHLMANNWILSDORF, D .
ACTA METALLURGICA ET MATERIALIA, 1992, 40 (02) :205-219
[6]   CHOICE OF COLLIMATORS FOR A CRYSTAL SPECTROMETER FOR NEUTRON DIFFRACTION [J].
CAGLIOTI, G ;
PAOLETTI, A ;
RICCI, FP .
NUCLEAR INSTRUMENTS & METHODS, 1958, 3 (04) :223-228
[7]   ON THE MICROSTRUCTURAL EVOLUTION OF COLD-ROLLED AL+5AT.PERCENT MG [J].
DIRRAS, GF ;
BIGET, MP ;
REY, C .
SCRIPTA METALLURGICA ET MATERIALIA, 1995, 33 (05) :755-760
[8]   Contrast factors of dislocations in the hexagonal crystal system [J].
Dragomir, IC ;
Ungár, T .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2002, 35 :556-564
[9]  
EICKHOFF K, 1953, Z METALLKD, V44, P223
[10]   Microhardness measurements and the Hall-Petch relationship in an Al-Mg alloy with submicrometer grain size [J].
Furukawa, M ;
Horita, Z ;
Nemoto, M ;
Valiev, RZ ;
Langdon, TG .
ACTA MATERIALIA, 1996, 44 (11) :4619-4629