Direct visualization of cubic to tetragonal phase transition in La0.2Sr0.8MnO3-δ using transmission electron microscopy

被引:2
作者
Shahee, Aga [1 ]
Lalla, Niranjan Prasad [1 ]
机构
[1] UGC DAE Consortium Sci Res, Indore 452001, Madhya Pradesh, India
关键词
Manganite; Coupled phase transition; Low temperature transmission electron microscopy; Low temperature x-ray diffraction; MANGANITES; CHARGE; MAGNETORESISTANCE; LA0.5CA0.5MNO3; DIFFRACTION; DIAGRAM;
D O I
10.1016/j.physb.2014.02.055
中图分类号
O469 [凝聚态物理学];
学科分类号
070205 ;
摘要
Structural phase transition studies employing low-temperature transmission electron microscopy (LT-TEM) and low-temperature x-ray diffraction (LT-XRD) have been carried out on wide-band La0.2Sr0.8MnO3-delta (delta=0.01) manganite. These studies reveal clear evidence of cubic to tetragonal phase transition occurring below 260 K in La0.2Sr0.8MnO3-delta (delta=0.01). TEM observations depict that cubic to tetragonal phase-transition results in formation of nanotwinned microstructure of the tetragonal phase. Formation of nanotwins has been attributed to orbital-orientation phase-separation leading to minimization of strain. The magnetic and electron transport measurements reveal that the structural phase transition is coupled with a canted C-type antiferromagnetic and semi-conductor to insulating phase transition. (C) 2014 Elsevier B.V. All rights reserved.
引用
收藏
页码:290 / 296
页数:7
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