On-line solid phase extraction system for chromium determination in water samples by flow injection-flame atomic absorption spectrometry

被引：43

作者：

Saracoglu, S

Soylak, M ^{[1
]}

Elci, L

机构：

[1] Erciyes Univ, Fac Art & Sci, Dept Chem, TR-38039 Kayseri, Turkey

[2] Pamukkale Univ, Fac Art & Sci, Dept Chem, TR-20020 Denizli, Turkey

来源：

ANALYTICAL LETTERS | 2002年 / 35卷 / 09期

关键词：

flow injection; solid phase extraction; preconcentration; separation; Chromotrope 2R coated Amberlite XAD-1180 resin;

D O I：

10.1081/AL-120006727

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

An on-line solid phase extraction system has been established for flow injection flame atomic absorption spectrometric determination of chromium on Chromotrope 2R coated Amberlite XAD-1180 (2R-1180) resin. Some parameters such as pH, flow rates of sample and elution solution, matrix effects on the quantitative recoveries of chromium from the resin were examined. The detection limit (3sigma) was 2.59 mug/L for preconcentration at 6.5 mL/min. The method was applied for the determination of traces chromium in natural water samples with satisfactory results (relative standard deviations below 5%, recoveries >95%).

引用

页码：1519 / 1530

页数：12

共 50 条

[41] On-line filtration system for determining total chromium and chromium in the soluble fraction of industrial effluents by flow injection flame atomic absorption spectrometry
López-García, I
Moreño, BM
Campillo, N
Hernández-Córdoba, M
ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2002, 373 (1-2) : 98 - 102
[42] Evaluation of Pb-Spec® for flow-injection solid-phase extraction preconcentration for the determination of trace lead in water and wine by flame atomic absorption spectrometry
Bakircioglu, Y
Segade, SR
Yourd, ER
Tyson, JF
ANALYTICA CHIMICA ACTA, 2003, 485 (01) : 9 - 18
[43] Determination of Zn(II) in alcohol fuel by flame atomic absorption spectrometry after on-line preconcentration using a solid phase extraction system
Alves, Vanessa N.
Mosquetta, Rafael
Carasek, Eduardo
Coelho, Nivia M. M.
JOURNAL OF ANALYTICAL CHEMISTRY, 2012, 67 (05) : 448 - 454
[44] Determination of Zn(II) in alcohol fuel by flame atomic absorption spectrometry after on-line preconcentration using a solid phase extraction system
Vanessa N. Alves
Rafael Mosquetta
Eduardo Carasek
Nívia M. M. Coelho
Journal of Analytical Chemistry, 2012, 67 : 448 - 454
[45] Determination of Gold by Solid Phase Extraction and Flame Atomic Absorption Spectrometry
Li, Hongwei
Huang, Zhangjie
Li, Weiqun
ASIAN JOURNAL OF CHEMISTRY, 2012, 24 (11) : 5003 - 5005
[46] Determination of Lead in Water Using Amber lite XAD-2 Functionalized With Xylenol Orange Resin as Column Material for On-line Flow Injection-Flame Atomic Absorption Spectrometry Analysis
Saxena, Reena
Saxena, Suneeti
Sarojam, Praveen
ATOMIC SPECTROSCOPY, 2012, 33 (03) : 83 - 91
[47] On-line bidirectional electrostacking of chromium(III) and chromium(VI) for flame atomic absorption spectrometry determination
He, YZ
Cervera, ML
Garrido-Ecija, MI
de la Guardia, M
ANALYTICA CHIMICA ACTA, 2000, 421 (01) : 57 - 65
[48] Simultaneous preconcentration of cadmium and chromium(III) in water samples by cloud point extraction and their determination by flame atomic absorption spectrometry
Meng, Lifen
Ning, Jinyan
Yang, Yaling
WATER SCIENCE AND TECHNOLOGY, 2014, 70 (12) : 1913 - 1918
[49] Flow injection on-line displacement sorption preconcentration coupled with flame atomic absorption spectrometry for the determination of trace lead in biological samples
Han De-Man
Jia Wen-Ping
Liang Hua-Ding
Yan Xiu-Ping
CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2007, 35 (11) : 1643 - 1646
[50] Indirect Determination of Sulfadiazine by Cloud Point Extraction/Flow Injection-Flame Atomic Absorption (CPE/FI-FAAS) Spectrometry
Dadfarnia, Shayessteh
Hajishabani, All Mohammad
Rad, Hamid Fazeli
JOURNAL OF THE CHINESE CHEMICAL SOCIETY, 2011, 58 (04) : 503 - 508

← 1 2 3 4 5 →